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This Special Issue, “Research as a Development Perspective”, is dedicated to data presented at the first Conference in Chemistry for Graduate/Postgraduate Students and PhD candidates at Aristotle University of Thessaloniki, which was the outcome of research conducted by young chemists in Northern Greece. The conference was organized by the Chemistry Department at Aristotle University of Thessaloniki, the Association of Greek Chemists-Division of Central and Western Macedonia, and the Association of Chemists in Northern Greece. The scope of this conference was to provide young chemists (but also last year’s students) with the opportunity to be well prepared for their next career steps in an increasingly demanding job market. Moreover, they had the possibility of presenting their scientific results to a large audience, which strengthened their soft skills. Lastly, the active engagement of students in the organization of the conference enhanced their teamwork abilities, a highly valuable when developing professional maturity.
HPLC-DAD --- bisphenol A --- 4-Hydroxybenzoic Acid --- 4-Hydroxyacetophenone hydroquinone --- Lactococcus lactis --- reversed-phase liquid chromatography --- ionizable and non-ionizable analytes --- isocratic and gradient elution in different eluent pHs --- computer-assisted separation optimization --- visualization of predicted chromatograms --- silk fibroin --- drug delivery --- magnetic silk fibroin --- bovine serum albumin --- food --- sample preparation techniques --- sulfonamides --- high-performance liquid chromatography --- HPLC --- ultra-high-performance liquid chromatography --- UHPLC --- Derveni --- Ancient Macedonia --- micro-XRF --- XRD --- HS-SPME/GC-MS --- ancient medicines --- ancient pharmaceuticals --- shellfish purple --- porphyra --- high-tin bronzes --- bronzes --- phosphorus --- boron --- inductively coupled plasma --- atomic emission spectrometry --- fertilizers --- acid dissolution --- wet digestion --- NSAIDs --- derivatization --- GC-MS --- serum
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This Special Issue, “Research as a Development Perspective”, is dedicated to data presented at the first Conference in Chemistry for Graduate/Postgraduate Students and PhD candidates at Aristotle University of Thessaloniki, which was the outcome of research conducted by young chemists in Northern Greece. The conference was organized by the Chemistry Department at Aristotle University of Thessaloniki, the Association of Greek Chemists-Division of Central and Western Macedonia, and the Association of Chemists in Northern Greece. The scope of this conference was to provide young chemists (but also last year’s students) with the opportunity to be well prepared for their next career steps in an increasingly demanding job market. Moreover, they had the possibility of presenting their scientific results to a large audience, which strengthened their soft skills. Lastly, the active engagement of students in the organization of the conference enhanced their teamwork abilities, a highly valuable when developing professional maturity.
Research & information: general --- HPLC-DAD --- bisphenol A --- 4-Hydroxybenzoic Acid --- 4-Hydroxyacetophenone hydroquinone --- Lactococcus lactis --- reversed-phase liquid chromatography --- ionizable and non-ionizable analytes --- isocratic and gradient elution in different eluent pHs --- computer-assisted separation optimization --- visualization of predicted chromatograms --- silk fibroin --- drug delivery --- magnetic silk fibroin --- bovine serum albumin --- food --- sample preparation techniques --- sulfonamides --- high-performance liquid chromatography --- HPLC --- ultra-high-performance liquid chromatography --- UHPLC --- Derveni --- Ancient Macedonia --- micro-XRF --- XRD --- HS-SPME/GC-MS --- ancient medicines --- ancient pharmaceuticals --- shellfish purple --- porphyra --- high-tin bronzes --- bronzes --- phosphorus --- boron --- inductively coupled plasma --- atomic emission spectrometry --- fertilizers --- acid dissolution --- wet digestion --- NSAIDs --- derivatization --- GC-MS --- serum --- HPLC-DAD --- bisphenol A --- 4-Hydroxybenzoic Acid --- 4-Hydroxyacetophenone hydroquinone --- Lactococcus lactis --- reversed-phase liquid chromatography --- ionizable and non-ionizable analytes --- isocratic and gradient elution in different eluent pHs --- computer-assisted separation optimization --- visualization of predicted chromatograms --- silk fibroin --- drug delivery --- magnetic silk fibroin --- bovine serum albumin --- food --- sample preparation techniques --- sulfonamides --- high-performance liquid chromatography --- HPLC --- ultra-high-performance liquid chromatography --- UHPLC --- Derveni --- Ancient Macedonia --- micro-XRF --- XRD --- HS-SPME/GC-MS --- ancient medicines --- ancient pharmaceuticals --- shellfish purple --- porphyra --- high-tin bronzes --- bronzes --- phosphorus --- boron --- inductively coupled plasma --- atomic emission spectrometry --- fertilizers --- acid dissolution --- wet digestion --- NSAIDs --- derivatization --- GC-MS --- serum
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Nature has always been, and still is, a source of food and ingredients that are beneficial to human health. Nowadays, plant extracts are increasingly becoming important additives in the food industry due to their antimicrobial and antioxidant activities that delay the development of off-flavors and improve the shelf life and color stability of food products. Due to their natural origin, they are excellent candidates to replace synthetic compounds, which are generally considered to have toxicological and carcinogenic effects. The efficient extraction of these compounds from their natural sources and the determination of their activity in commercialized products have been great challenges for researchers and food chain contributors to develop products with positive effects on human health. The objective of this Special Issue is to highlight the existing evidence regarding the various potential benefits of the consumption of plant extracts and plant-extract-based products, with emphasis on in vivo works and epidemiological studies, the application of plant extracts to improving shelf life, the nutritional and health-related properties of foods, and the extraction techniques that can be used to obtain bioactive compounds from plant extracts.
Research & information: general --- Biology, life sciences --- Food & society --- gut microbiota --- natural products --- diabetes mellitus --- complications --- mechanisms --- pepper --- fermentation --- hyperglycemia --- angiotensin I-converting enzyme (ACE) inhibition --- antioxidant --- Berberis --- food preservative --- alkaloid --- human health --- andrographolide --- reversed-phase liquid chromatography --- quantitative analysis --- method validation --- anti-inflammatory activity --- phenolic acids --- emulsions --- antioxidants --- health properties --- multidrug resistance --- doxorubicin --- MRSA --- quorum sensing --- biofilm --- rice bran --- polyphenols --- oxidative stress --- inflammation --- anti-inflammatory --- Sideritis raeseri subsp. raeseri --- essential oil --- antimicrobial --- antiproliferative activity --- Euphorbia hirta L. --- bioactive compounds --- in vitro α-amylase inhibition --- streptozotocin-induced diabetic mice --- Jujube --- hydrolysis --- anti-inflammation --- lung --- NF-κB --- Nrf2 --- HO-1 --- Kadsura spp. --- fruit parts --- phenolics --- antioxidant capacity --- in vitro health properties --- bud-derivatives --- botanicals --- UV-Visible spectroscopic fingerprint --- chemometrics --- targeted chromatographic fingerprint --- tomato pomace --- extraction --- platelet --- ultrasound --- functional ingredient --- gut microbiota --- natural products --- diabetes mellitus --- complications --- mechanisms --- pepper --- fermentation --- hyperglycemia --- angiotensin I-converting enzyme (ACE) inhibition --- antioxidant --- Berberis --- food preservative --- alkaloid --- human health --- andrographolide --- reversed-phase liquid chromatography --- quantitative analysis --- method validation --- anti-inflammatory activity --- phenolic acids --- emulsions --- antioxidants --- health properties --- multidrug resistance --- doxorubicin --- MRSA --- quorum sensing --- biofilm --- rice bran --- polyphenols --- oxidative stress --- inflammation --- anti-inflammatory --- Sideritis raeseri subsp. raeseri --- essential oil --- antimicrobial --- antiproliferative activity --- Euphorbia hirta L. --- bioactive compounds --- in vitro α-amylase inhibition --- streptozotocin-induced diabetic mice --- Jujube --- hydrolysis --- anti-inflammation --- lung --- NF-κB --- Nrf2 --- HO-1 --- Kadsura spp. --- fruit parts --- phenolics --- antioxidant capacity --- in vitro health properties --- bud-derivatives --- botanicals --- UV-Visible spectroscopic fingerprint --- chemometrics --- targeted chromatographic fingerprint --- tomato pomace --- extraction --- platelet --- ultrasound --- functional ingredient
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In this Topical Collection, ten articles (one review and nine research articles) are published in a time span of 2021–2022. All articles are written by experts in the field of Separation Techniques who were invited to contribute to the presentation of the current status in separation science. The authors were invited to answer the questions: What is the state-of-the-art in Separation Sciences? What advances have been reported recently? Last but not least, what are the future perspectives? The Editor and authors hope that the readers will find valuable information in the topic.
Research & information: general --- Chemistry --- protein-based chiral stationary phase --- alpha 1-acid glycoprotein --- chiral recognition mechanism --- molecular docking --- proteomics --- high-performance liquid chromatography --- mass spectrometry --- gout --- uric acid --- Salvia miltiorrhiza --- HPLC-MS/MS --- pharmacokinetics --- wine-processed --- hydrophilic interaction liquid chromatography --- chromatography --- oligopeptides --- acetyl hexapeptide-8 --- acetyl hexapeptide-3 --- Argireline --- cosmetics --- SARS-CoV-2 --- virus particles --- air filtering --- aerosols --- probability distributions --- rotational particle separator --- air separation --- steam methane reforming --- water gas shift --- alternative fluids --- gas turbine --- Senecio anteuphorbium --- response factors --- true quantitation --- allelopathy --- herbicide --- chlorpropham --- potato --- μQuEChERS/UHPLC-PDA --- validation --- cooking --- methyl nicotinate --- methyl salicylate --- ethyl salicylate --- 2-hydroxyethyl salicylate --- pain relief spray --- Tulasnellaceae sp. --- Gymnadenia orchidis --- mdium-pressure liquid chromatography --- reversed-phase liquid chromatography --- ergosterol
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In the field of Analytical Chemistry and, in particular, whenever a quali-quantitative analysis is required, until a few years ago, reference was made exclusively to instrumental methods (more or less hyphenated) which, once validated, were able to provide the answers to the questions present, even if only in a limited way to analytical targets. Nowadays, the landscape has become considerably complicated (natural adulterants, assessment of geographical origin, sophistication, need for non-destructive analysis, search for often unknown compounds), and new procedures for processing data have greatly increased the potential of analyses that are conducted (even routinely) in the laboratory. In this scenario, chemometrics is master, able to manage and process a huge amount of information based both on data relating only to the analytes of interest, but also by applying “general” procedures to process raw untargeted analysis data. It is within this strand of analysis that many of the works reported in this Special Issue fall. In the succession of works in this printed version, the criterion that guided us was to highlight how—starting exclusively from chromatographic techniques (HPLC and GC) with conventional detectors and moving to exclusively spectroscopic techniques (MS, FT-IR and Raman)—it is possible arrive at extremely powerful coupled techniques and procedures (HPLC and FT-IR) able to meet research needs. Finally, at the end of the printed volume, there are two reviews that surveying the state of the art regarding the assessment of authenticity through qualitative analyses and the application of chemometrics in the pharmaceutical field in the study of forced drug degradation products. From the succession of works (and, above all, from the various application fields) it can immediately be seen how the application of chemometrics and its procedures to both raw and processed data is a powerful means of obtaining robust, reproducible, and predictive information. In this manner, it is possible to create models able to explain and respond to the original problem in a much more detailed way. , and Honghe through Fourier transform mid infrared (FT-MIR) spectra combined with partial least squares discriminant analysis (PLS-DA), random forest (RF), and hierarchical cluster analysis (HCA) methods. Melucci and collaborators apply chemometric approaches to non-destructive analysis of ATR-FT-IR for the determination of biosilica content. This value was directly evaluated in sediment samples, without any chemical alteration, using attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy, and the quantification was performed by combining the multivariate standard addition method (MSAM) with the net analyte signal (NAS) procedure to solve the strong matrix effect of sediment samples. Still in the food and food supplements field, Anguebes-Franseschi and collaborators report an article where 10 chemometric models based on Raman spectroscopy were applied to predict the physicochemical properties of honey produced in the state of Campeche, Mexico.
Medicine --- Paris polyphylla Smith var. yunnanensis --- multivariate analysis --- chemometrics --- Fourier transform infrared --- amino acids --- reversed-phase liquid chromatography --- gradient elution --- retention prediction --- artificial neural network --- Macrohyporia cocos --- data fusion --- liquid chromatography --- fourier transform infrared spectroscopy --- partial least squares discriminant analysis --- authentication --- Gastrodia elata tuber --- quality evaluation --- HPLC --- QAMS --- Ranae Oviductus --- identification --- protein --- RP-HPLC --- fingerprint --- fish and seafood --- food authentication --- fingerprinting --- wild and farmed --- geographical origin --- vibrational spectroscopy --- absorption/fluorescence spectroscopy --- nuclear magnetic resonance --- hyperspectral imaging --- saffron --- adulteration --- food authenticity --- gas-chromatography --- eupatorin --- UHPLC-Q-TOF-MS/MS --- metabolism --- in vivo and in vitro --- rat liver microsomes --- rat intestinal flora --- untargeted metabolomics --- PARAFAC2 --- alignment --- gas chromatography–mass spectrometry (GC–MS) --- prostate carcinoma --- forced degradation --- degradation products --- stress test --- diatoms --- biogenic silica --- ATR-FTIR --- NAS --- quality control --- Raman spectroscopy --- honey --- PLS regression models --- physicochemical parameters
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Nature has always been, and still is, a source of food and ingredients that are beneficial to human health. Nowadays, plant extracts are increasingly becoming important additives in the food industry due to their antimicrobial and antioxidant activities that delay the development of off-flavors and improve the shelf life and color stability of food products. Due to their natural origin, they are excellent candidates to replace synthetic compounds, which are generally considered to have toxicological and carcinogenic effects. The efficient extraction of these compounds from their natural sources and the determination of their activity in commercialized products have been great challenges for researchers and food chain contributors to develop products with positive effects on human health. The objective of this Special Issue is to highlight the existing evidence regarding the various potential benefits of the consumption of plant extracts and plant-extract-based products, with emphasis on in vivo works and epidemiological studies, the application of plant extracts to improving shelf life, the nutritional and health-related properties of foods, and the extraction techniques that can be used to obtain bioactive compounds from plant extracts.
gut microbiota --- natural products --- diabetes mellitus --- complications --- mechanisms --- pepper --- fermentation --- hyperglycemia --- angiotensin I-converting enzyme (ACE) inhibition --- antioxidant --- Berberis --- food preservative --- alkaloid --- human health --- andrographolide --- reversed-phase liquid chromatography --- quantitative analysis --- method validation --- anti-inflammatory activity --- phenolic acids --- emulsions --- antioxidants --- health properties --- multidrug resistance --- doxorubicin --- MRSA --- quorum sensing --- biofilm --- rice bran --- polyphenols --- oxidative stress --- inflammation --- anti-inflammatory --- Sideritis raeseri subsp. raeseri --- essential oil --- antimicrobial --- antiproliferative activity --- Euphorbia hirta L. --- bioactive compounds --- in vitro α-amylase inhibition --- streptozotocin-induced diabetic mice --- Jujube --- hydrolysis --- anti-inflammation --- lung --- NF-κB --- Nrf2 --- HO-1 --- Kadsura spp. --- fruit parts --- phenolics --- antioxidant capacity --- in vitro health properties --- bud-derivatives --- botanicals --- UV-Visible spectroscopic fingerprint --- chemometrics --- targeted chromatographic fingerprint --- tomato pomace --- extraction --- platelet --- ultrasound --- functional ingredient --- n/a
Choose an application
In the field of Analytical Chemistry and, in particular, whenever a quali-quantitative analysis is required, until a few years ago, reference was made exclusively to instrumental methods (more or less hyphenated) which, once validated, were able to provide the answers to the questions present, even if only in a limited way to analytical targets. Nowadays, the landscape has become considerably complicated (natural adulterants, assessment of geographical origin, sophistication, need for non-destructive analysis, search for often unknown compounds), and new procedures for processing data have greatly increased the potential of analyses that are conducted (even routinely) in the laboratory. In this scenario, chemometrics is master, able to manage and process a huge amount of information based both on data relating only to the analytes of interest, but also by applying “general” procedures to process raw untargeted analysis data. It is within this strand of analysis that many of the works reported in this Special Issue fall. In the succession of works in this printed version, the criterion that guided us was to highlight how—starting exclusively from chromatographic techniques (HPLC and GC) with conventional detectors and moving to exclusively spectroscopic techniques (MS, FT-IR and Raman)—it is possible arrive at extremely powerful coupled techniques and procedures (HPLC and FT-IR) able to meet research needs. Finally, at the end of the printed volume, there are two reviews that surveying the state of the art regarding the assessment of authenticity through qualitative analyses and the application of chemometrics in the pharmaceutical field in the study of forced drug degradation products. From the succession of works (and, above all, from the various application fields) it can immediately be seen how the application of chemometrics and its procedures to both raw and processed data is a powerful means of obtaining robust, reproducible, and predictive information. In this manner, it is possible to create models able to explain and respond to the original problem in a much more detailed way. , and Honghe through Fourier transform mid infrared (FT-MIR) spectra combined with partial least squares discriminant analysis (PLS-DA), random forest (RF), and hierarchical cluster analysis (HCA) methods. Melucci and collaborators apply chemometric approaches to non-destructive analysis of ATR-FT-IR for the determination of biosilica content. This value was directly evaluated in sediment samples, without any chemical alteration, using attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy, and the quantification was performed by combining the multivariate standard addition method (MSAM) with the net analyte signal (NAS) procedure to solve the strong matrix effect of sediment samples. Still in the food and food supplements field, Anguebes-Franseschi and collaborators report an article where 10 chemometric models based on Raman spectroscopy were applied to predict the physicochemical properties of honey produced in the state of Campeche, Mexico.
Paris polyphylla Smith var. yunnanensis --- multivariate analysis --- chemometrics --- Fourier transform infrared --- amino acids --- reversed-phase liquid chromatography --- gradient elution --- retention prediction --- artificial neural network --- Macrohyporia cocos --- data fusion --- liquid chromatography --- fourier transform infrared spectroscopy --- partial least squares discriminant analysis --- authentication --- Gastrodia elata tuber --- quality evaluation --- HPLC --- QAMS --- Ranae Oviductus --- identification --- protein --- RP-HPLC --- fingerprint --- fish and seafood --- food authentication --- fingerprinting --- wild and farmed --- geographical origin --- vibrational spectroscopy --- absorption/fluorescence spectroscopy --- nuclear magnetic resonance --- hyperspectral imaging --- saffron --- adulteration --- food authenticity --- gas-chromatography --- eupatorin --- UHPLC-Q-TOF-MS/MS --- metabolism --- in vivo and in vitro --- rat liver microsomes --- rat intestinal flora --- untargeted metabolomics --- PARAFAC2 --- alignment --- gas chromatography–mass spectrometry (GC–MS) --- prostate carcinoma --- forced degradation --- degradation products --- stress test --- diatoms --- biogenic silica --- ATR-FTIR --- NAS --- quality control --- Raman spectroscopy --- honey --- PLS regression models --- physicochemical parameters
Choose an application
In the field of Analytical Chemistry and, in particular, whenever a quali-quantitative analysis is required, until a few years ago, reference was made exclusively to instrumental methods (more or less hyphenated) which, once validated, were able to provide the answers to the questions present, even if only in a limited way to analytical targets. Nowadays, the landscape has become considerably complicated (natural adulterants, assessment of geographical origin, sophistication, need for non-destructive analysis, search for often unknown compounds), and new procedures for processing data have greatly increased the potential of analyses that are conducted (even routinely) in the laboratory. In this scenario, chemometrics is master, able to manage and process a huge amount of information based both on data relating only to the analytes of interest, but also by applying “general” procedures to process raw untargeted analysis data. It is within this strand of analysis that many of the works reported in this Special Issue fall. In the succession of works in this printed version, the criterion that guided us was to highlight how—starting exclusively from chromatographic techniques (HPLC and GC) with conventional detectors and moving to exclusively spectroscopic techniques (MS, FT-IR and Raman)—it is possible arrive at extremely powerful coupled techniques and procedures (HPLC and FT-IR) able to meet research needs. Finally, at the end of the printed volume, there are two reviews that surveying the state of the art regarding the assessment of authenticity through qualitative analyses and the application of chemometrics in the pharmaceutical field in the study of forced drug degradation products. From the succession of works (and, above all, from the various application fields) it can immediately be seen how the application of chemometrics and its procedures to both raw and processed data is a powerful means of obtaining robust, reproducible, and predictive information. In this manner, it is possible to create models able to explain and respond to the original problem in a much more detailed way. , and Honghe through Fourier transform mid infrared (FT-MIR) spectra combined with partial least squares discriminant analysis (PLS-DA), random forest (RF), and hierarchical cluster analysis (HCA) methods. Melucci and collaborators apply chemometric approaches to non-destructive analysis of ATR-FT-IR for the determination of biosilica content. This value was directly evaluated in sediment samples, without any chemical alteration, using attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy, and the quantification was performed by combining the multivariate standard addition method (MSAM) with the net analyte signal (NAS) procedure to solve the strong matrix effect of sediment samples. Still in the food and food supplements field, Anguebes-Franseschi and collaborators report an article where 10 chemometric models based on Raman spectroscopy were applied to predict the physicochemical properties of honey produced in the state of Campeche, Mexico.
Medicine --- Paris polyphylla Smith var. yunnanensis --- multivariate analysis --- chemometrics --- Fourier transform infrared --- amino acids --- reversed-phase liquid chromatography --- gradient elution --- retention prediction --- artificial neural network --- Macrohyporia cocos --- data fusion --- liquid chromatography --- fourier transform infrared spectroscopy --- partial least squares discriminant analysis --- authentication --- Gastrodia elata tuber --- quality evaluation --- HPLC --- QAMS --- Ranae Oviductus --- identification --- protein --- RP-HPLC --- fingerprint --- fish and seafood --- food authentication --- fingerprinting --- wild and farmed --- geographical origin --- vibrational spectroscopy --- absorption/fluorescence spectroscopy --- nuclear magnetic resonance --- hyperspectral imaging --- saffron --- adulteration --- food authenticity --- gas-chromatography --- eupatorin --- UHPLC-Q-TOF-MS/MS --- metabolism --- in vivo and in vitro --- rat liver microsomes --- rat intestinal flora --- untargeted metabolomics --- PARAFAC2 --- alignment --- gas chromatography–mass spectrometry (GC–MS) --- prostate carcinoma --- forced degradation --- degradation products --- stress test --- diatoms --- biogenic silica --- ATR-FTIR --- NAS --- quality control --- Raman spectroscopy --- honey --- PLS regression models --- physicochemical parameters --- Paris polyphylla Smith var. yunnanensis --- multivariate analysis --- chemometrics --- Fourier transform infrared --- amino acids --- reversed-phase liquid chromatography --- gradient elution --- retention prediction --- artificial neural network --- Macrohyporia cocos --- data fusion --- liquid chromatography --- fourier transform infrared spectroscopy --- partial least squares discriminant analysis --- authentication --- Gastrodia elata tuber --- quality evaluation --- HPLC --- QAMS --- Ranae Oviductus --- identification --- protein --- RP-HPLC --- fingerprint --- fish and seafood --- food authentication --- fingerprinting --- wild and farmed --- geographical origin --- vibrational spectroscopy --- absorption/fluorescence spectroscopy --- nuclear magnetic resonance --- hyperspectral imaging --- saffron --- adulteration --- food authenticity --- gas-chromatography --- eupatorin --- UHPLC-Q-TOF-MS/MS --- metabolism --- in vivo and in vitro --- rat liver microsomes --- rat intestinal flora --- untargeted metabolomics --- PARAFAC2 --- alignment --- gas chromatography–mass spectrometry (GC–MS) --- prostate carcinoma --- forced degradation --- degradation products --- stress test --- diatoms --- biogenic silica --- ATR-FTIR --- NAS --- quality control --- Raman spectroscopy --- honey --- PLS regression models --- physicochemical parameters
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