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The imminent challenge in geometallurgical characterization of today’s ore deposits is its inherent heterogeneity and complexity which demands fast, resource-efficient, robust, and cost-effective means of measurement and analysis. To address this concern, mining operations all over the world are incorporating SEM-based automated mineralogy systems. Next generation platforms have been developed to bring out these technologies from the laboratories unto the field for on-site mineralogical characterization. Its widespread use have established its significance in the mining industry, however, cross-validation of results between technologies has not been well studied. This study aims to compare and validate results gathered from two SEM platforms: the ZEISS SIGMA 300 Gemini (FEG) with the ZEISS MinSCAN (W-filament) both are coupled with the ZEISS Mineralogic Mining system. Three sets of mixed Cu ore samples (feed, concentrate, and tails) from the Kansanshi deposit were analyzed exploring the effects of SEM operating conditions and sample preparation. The work focused on comparison of the modal mineralogy. The quality of results were assessed by its repeatability and cross-validated with chemical assay (AR-AAS). The limitations of these SEM-based systems were defined and solutions were proposed involving correlative microscopy. The feasibility of employing machine learning algorithms in image classification techniques were proposed to improve data acquisition process and accuracy of results of automated mineralogy systems. This study establishes the effect of the mineral recipe or SIP to the accuracy of results of a quantitative mineralogical analysis. Expertise in the deposit mineralogy as well as in the capabilities and limitations of the SEM is crucial in achieving reliable results. Cross-validation of back-calculated Mineralogic Cu and Fe grades from modal mineralogy with the measured AR-AAS chemical analysis shows that the error is minimized with the ZEISS SIGMA on samples prepared using carbon black. However, it must be noted that not all numerical values can be directly compared between the results and should be treated merely as indications of accuracy. Combined features from images obtained from the optical microscope (RGB) and the SEM (BSE) showed the least error in classification using a support vector machine algorithm. The segmented image shows mineral domains where EDX analysis can be performed on a set amount of points veering away from the pixel-by-pixel full mapping acquisition mode. This methodology can be developed and applied to automated mineralogy image processing systems as a domain-based acquisition mode. This has the potential to improve quantitative mineralogical analysis results accuracy while reducing acquisition time and resource costs.
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In this project, the ore of the project of expansion of Draa Sfar mine is studied. The deposit is a Cu-Pb-Zn polymetallic Volcanogenic Massive Sulphide. The project extension contains three main ore-types: the polymetallic mineralisation from -1200 m to -1300 m, the polymetallic mineralisation from -1300 m to -1500 m and a copper-rich polymetallic ore. Targeted minerals are galena for lead, chalcopyrite for copper and sphalerite for zinc. The ores of the extension are first studied to determine its quantitative mineralogy. The ores of the deposit extension are compared to the ore that is presently exploited in Draa Sfar. Then, in a second stage, their behaviour is estimated in a laboratory flowsheet similar to the one of the the flotation plant used to process the ore currently extracted from Draa Sfar mine called reference ore. The flowsheet comprises multiple grinding stages in between a lead, a copper and finally a zinc flotation circuits. To fulfil both objectives, the three ores of the extension project and the present ore are sampled and analysed. Then, they are floated in laboratory tests and their products are analysed on bulk and sized samples, SEM is also used. A sampling of the plant is also conducted, but on a too short period to provide reliable results. Ores of the extension project appear poorer in lead and zinc than reference ore, they are also richer in copper. In the lower part of the deposit, -1200 m, the liberation degree of galena is decreasing and the one of chalcopyrite increasing compared to the reference ore. These characteristics of the future feed of the plant suggest to modify the flowsheet to a copper flotation followed by lead and zinc flotations. At laboratory scale, the reference ore produces lead, copper and zinc concentrates with higher recoveries than in the ores of the extension project. In the lead, copper and zinc circuit, the concentrates are diluted by an entrainment of sulphide and silicate gangue pointing to a lack of selectivity of the three flotation circuits. In the lead circuit, the low recoveries in the concentrates of the ores of the extension project compared to reference ore can be related to a lack of liberation of galena leading to losses to the middling streams of the copper circuit. In the copper concentrate, copper grade is higher in ores from the extension thanks to the coarser liberation of chalcopyrite in the reference.
Cu-Pb-Zn polymetallic ores, quantitative mineralogy, process mineralogy, geometallurgy, flotation, laboratory test, laboratory scale, plant scale, sampling, masse balance, size by size study, SEM, liberation degree, mineral associations, sulphide gangue --- Ingénierie, informatique & technologie > Géologie, ingénierie du pétrole & des mines
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This Special Issue, focusing on the value of mineralogical monitoring for the mining and minerals industry, should include detailed investigations and characterizations of minerals and ores of the following fields for ore and process control: Lithium ores—determination of lithium contents by XRD methods; Copper ores and their different mineralogy; Nickel lateritic ores; Iron ores and sinter; Bauxite and bauxite overburden; Heavy mineral sands. The value of quantitative mineralogical analysis, mainly by XRD methods, combined with other techniques for the evaluation of typical metal ores and other important minerals, will be shown and demonstrated for different minerals. The different steps of mineral processing and metal contents bound to different minerals will be included. Additionally, some processing steps, mineral enrichments, and optimization of mineral determinations using XRD will be demonstrated. Statistical methods for the treatment of a large set of XRD patterns of ores and mineral concentrates, as well as their value for the characterization of mineral concentrates and ores, will be demonstrated. Determinations of metal concentrations in minerals by different methods will be included, as well as the direct prediction of process parameters from raw XRD data.
Technology: general issues --- History of engineering & technology --- Mining technology & engineering --- barite --- mineralogy --- industrial application --- beneficiation --- specific gravity --- bauxite overburden --- Belterra Clay --- mineralogical quantification --- Rietveld analysis --- machine learning --- artificial intelligence --- mining --- mineralogical analysis --- bauxite --- available alumina --- reactive silica --- XRD --- PLSR --- lithium --- quantification --- clustering --- Rietveld --- cluster analysis --- spodumene --- petalite --- lepidolite --- triphylite --- zinnwaldite --- amblygonite --- chalcopyrite --- ore blending --- copper flotation --- nickel laterite --- ore sorting --- framboidal pyrite --- sulfide minerals --- flotation --- process mineralogy --- heavy minerals --- ilmenite --- titania slag --- rietveld --- Magneli phases --- n/a
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This Special Issue, focusing on the value of mineralogical monitoring for the mining and minerals industry, should include detailed investigations and characterizations of minerals and ores of the following fields for ore and process control: Lithium ores—determination of lithium contents by XRD methods; Copper ores and their different mineralogy; Nickel lateritic ores; Iron ores and sinter; Bauxite and bauxite overburden; Heavy mineral sands. The value of quantitative mineralogical analysis, mainly by XRD methods, combined with other techniques for the evaluation of typical metal ores and other important minerals, will be shown and demonstrated for different minerals. The different steps of mineral processing and metal contents bound to different minerals will be included. Additionally, some processing steps, mineral enrichments, and optimization of mineral determinations using XRD will be demonstrated. Statistical methods for the treatment of a large set of XRD patterns of ores and mineral concentrates, as well as their value for the characterization of mineral concentrates and ores, will be demonstrated. Determinations of metal concentrations in minerals by different methods will be included, as well as the direct prediction of process parameters from raw XRD data.
barite --- mineralogy --- industrial application --- beneficiation --- specific gravity --- bauxite overburden --- Belterra Clay --- mineralogical quantification --- Rietveld analysis --- machine learning --- artificial intelligence --- mining --- mineralogical analysis --- bauxite --- available alumina --- reactive silica --- XRD --- PLSR --- lithium --- quantification --- clustering --- Rietveld --- cluster analysis --- spodumene --- petalite --- lepidolite --- triphylite --- zinnwaldite --- amblygonite --- chalcopyrite --- ore blending --- copper flotation --- nickel laterite --- ore sorting --- framboidal pyrite --- sulfide minerals --- flotation --- process mineralogy --- heavy minerals --- ilmenite --- titania slag --- rietveld --- Magneli phases --- n/a
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This Special Issue, focusing on the value of mineralogical monitoring for the mining and minerals industry, should include detailed investigations and characterizations of minerals and ores of the following fields for ore and process control: Lithium ores—determination of lithium contents by XRD methods; Copper ores and their different mineralogy; Nickel lateritic ores; Iron ores and sinter; Bauxite and bauxite overburden; Heavy mineral sands. The value of quantitative mineralogical analysis, mainly by XRD methods, combined with other techniques for the evaluation of typical metal ores and other important minerals, will be shown and demonstrated for different minerals. The different steps of mineral processing and metal contents bound to different minerals will be included. Additionally, some processing steps, mineral enrichments, and optimization of mineral determinations using XRD will be demonstrated. Statistical methods for the treatment of a large set of XRD patterns of ores and mineral concentrates, as well as their value for the characterization of mineral concentrates and ores, will be demonstrated. Determinations of metal concentrations in minerals by different methods will be included, as well as the direct prediction of process parameters from raw XRD data.
Technology: general issues --- History of engineering & technology --- Mining technology & engineering --- barite --- mineralogy --- industrial application --- beneficiation --- specific gravity --- bauxite overburden --- Belterra Clay --- mineralogical quantification --- Rietveld analysis --- machine learning --- artificial intelligence --- mining --- mineralogical analysis --- bauxite --- available alumina --- reactive silica --- XRD --- PLSR --- lithium --- quantification --- clustering --- Rietveld --- cluster analysis --- spodumene --- petalite --- lepidolite --- triphylite --- zinnwaldite --- amblygonite --- chalcopyrite --- ore blending --- copper flotation --- nickel laterite --- ore sorting --- framboidal pyrite --- sulfide minerals --- flotation --- process mineralogy --- heavy minerals --- ilmenite --- titania slag --- rietveld --- Magneli phases
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