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Book
Modern Sample Preparation Approaches for Separation Science
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ISBN: 3039214128 303921411X Year: 2019 Publisher: MDPI - Multidisciplinary Digital Publishing Institute

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Abstract

This book will provide the most recent knowledge and advances in Sample Preparation Techniques for Separation Science. Everyone working in a laboratory must be familiar with the basis of these technologies, and they often involve elaborate and time-consuming procedures that can take up to 80% of the total analysis time. Sample preparation is an essential step in most of the analytical methods for environmental and biomedical analysis, since the target analytes are often not detected in their in-situ forms, or the results are distorted by interfering species. In the past decade, modern sample preparation techniques have aimed to comply with green analytical chemistry principles, leading to simplification, miniaturization, easy manipulation of the analytical devices, low costs, strong reduction or absence of toxic organic solvents, as well as low sample volume requirements.Modern Sample Preparation Approaches for Separation Science also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and forensic sciences.

Keywords

caffeine and acetaminophen tracers --- solvent delivery with a moving pipette --- determination --- China herbal tea --- enrichment --- review --- on-line --- pectin --- nanocomposite --- Cassiae Semen --- environmental analysis --- pathogenic --- preconcentration --- nail --- liver --- extraction --- sample preparation --- hydrogel --- solid-phase extraction --- geological samples --- ionic liquids --- rice grains --- subzero-temperature assisted liquid–liquid extraction --- sugaring-out assisted liquid–liquid extraction --- poly (OMA-co-TRIM) monolithic column --- hormones --- vortex-synchronized matrix solid-phase dispersion --- trace analysis --- gas chromatography --- LC–MS/MS --- membrane-based microextraction --- gold --- antipsychotics --- in-line filter --- HPLC --- space instrumentation --- liquid chromatography --- biological samples --- vitamins --- polyvinyl alcohol --- in-tube SPME --- high-frequency heating --- UPLC-MS/MS --- oxylipins --- nucleic acid isolation --- non-anthocyanin polyphenol --- large volume --- barbiturates --- solvent front position extraction --- oligopeptides --- urine --- SPE --- whole blood --- anthraquinones --- flow rate --- chlorophenoxy acid herbicides --- amlodipine --- schizophrenic’ patients --- salting-out assisted liquid–liquid extraction --- automation --- sorbent --- whole water --- blueberry --- hydrophobic-solvent assisted liquid–liquid extraction --- crab shells --- miniaturization --- curie temperature --- sand --- UHPLC-MS/MS --- multi-spheres adsorptive micro-extraction (MSA?E) --- floating sampling technology --- protein precipitation --- pesticides residue --- sample preparation with TLC/HPTLC --- phenolic compounds --- response surface methodology --- vortex-assisted dispersive liquid-liquid microextraction --- trapping system --- caffeine --- aflatoxins --- liquid chromatography–tandem mass spectrometry --- pesticides --- organic-based monoliths --- matrix solid phase dispersion --- simultaneous determination --- pharmaceuticals --- sorbent-based techniques --- desirability function approach --- plasma samples --- environmental water matrices --- hydrophobic in-tube solid-phase microextraction --- liquid–liquid extraction

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