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Although the seminal work of Fujishima et al. dates back to 1971, TiO2 still remains the most diffused and studied semiconductor, employed in photo-oxidation processes for cleantech (i.e., polluted water and air treatment), in solar fuel production (mainly hydrogen production by water photo splitting), and in Carbon Capture and Utilization (CCU) processes by CO2 photoreduction. The eleven articles, among them three reviews, in this book cover recent results and research trends of various aspects of titanium dioxide photocatalysis, with the chief aim of improving the final efficiency of TiO2-based materials. Strategies include doping, metal co-catalyst deposition, and the realization of composites with plasmonic materials, other semiconductors, and graphene. Photocatalysts with high efficiency and selectivity can be also obtained by controlling the precise crystal shape (and homogeneous size) and the organization in superstructures from ultrathin films to hierarchical nanostructures. Finally, the theoretical modeling of TiO2 nanoparticles is discussed and highlighted. The range of topics addressed in this book will stimulate the reader’s interest as well as provide a valuable source of information for researchers in academia and industry.

UV-visible --- n/a --- oxidative reaction systems --- photodegradation --- nanospheres --- heterojunction --- Ag/AgCl@TiO2 fibers --- polymorphism --- XRD --- copper-modified titania --- ultrasonic vibration --- brookite --- TiO2 modification --- simulated Extended X-ray Adsorption Fine-Structure (EXAFS) --- nanorod spheres --- trapped electrons --- flame-spray pyrolysis --- titania/water interface --- microwave irradiation --- plasmonic photocatalyst --- graphene-TiO2 --- photocatalytic hydrogen production --- microstreaming --- B3LYP --- HRTEM --- hardness --- printing and dyeing wastewater --- SCC-DFTB --- TiO2 --- photoelectrochemistry --- titanium --- bulk defects --- methanol photo-steam reforming --- spray coating --- sol-gel --- FTIR --- S-doping --- photocatalysis --- sulfidation --- lattice defects --- polymorph --- anodization --- pine-cone TiO2 nanoclusters --- nanorod arrays --- formation mechanism --- Cu and Pt nanoparticles --- excitons --- TiO2 nanotubes --- adhesion --- trapping --- flexible substrates --- optical absorption --- large-sized films --- surface defects --- titanium dioxide --- accumulated electrons

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Photoactive nanomaterials have been receiving increasing attention due to their potential application in the light-driven degradation of water and gas-phase pollutants. However, to exploit the great potential of photoactive materials and access their properties requires fine-tuning of their size/shape-dependent chemical–physical properties, and on the ability to integrate them in photoreactors or to deposit them onto large surfaces. Therefore, the synthetic approach as well as post-synthesis manipulation could strongly affect the final photocatalytic properties of the nanomaterial. The aim of the present Special Issue is to report on the most recent progress towards the application of photoactive nanomaterials and nanomaterial-based coatings in pollutant degradation, paying particular attention to cases close to real application: scalable synthetic approaches to nanocatalysts, preparation of nanocatalyst-based coatings, degradation of real pollutants and bacterial inactivation, and application in building materials.

toxicity --- polar herbicide --- composite nanorods --- heterojunction --- degradation --- nanocomposites --- nanoparticles --- polyester --- TiO2 nanotube --- environmental remediation --- building materials --- hydroxyapatite --- VOCs --- reactive green 12 --- Pt loaded TiO2 --- nanomaterials --- expansion --- photocatalytic activity --- CuxO/TiO2 --- water remediation --- antimicrobial properties --- sputtering --- diclofenac --- mesoporous --- TiO2 --- advanced oxidation processes --- mortar --- disinfection --- HiPIMS --- microcracks --- Cu2O --- sulfate attack --- NOx --- photocatalysis --- blast furnace slag --- paraquat --- recalcitrant pollutants --- shell thickness --- water treatments --- visible light LEDs --- cement --- deterioration --- transformation products --- gas-phase pollutants --- titanium dioxide --- photoelectrocatalysis --- Z-scheme

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Water pollution from biorefractory pollutants and emerging contaminants is still a very relevant problem worldwide. Examples of these pollutants include disinfection by-products, pharmaceutical and personal care products, persistent organic chemicals, as well as their degradation products. The occurrence of these contaminants in water has raised increasing concern due to their accumulation and persistence in the environment and the threat they pose to the ecological system and human health. In this Special Issue, papers regarding the advancements in materials and processes for use in the electro- and photoelectrochemical removal of different pollutants from water are collected. The synthesis, characterization and application of materials for use in electrochemical or photoelectrochemical techniques are presented, as well as studies concerning catalytic processes and reaction kinetics.

Technology: general issues --- Chemical engineering --- Au-TiO2 --- antibiotics --- emergent contaminants --- nanocatalyst --- photocatalysis --- GFN-xTB --- ibuprofen --- advanced oxidation process --- TiO2 --- active glass --- heterojunction --- charge separation --- chlorpyrifos --- photodegradation --- nanoparticles --- gold --- cyclodextrins --- perfluorooctanoic acid --- emerging contaminant --- defluorination --- platinum --- electro-oxidation --- strontium carbonate (SrCO3) --- solvothermal method --- visible light --- diethyl phthalate --- photoelectrochemical degradation --- persistent organic pollutants --- chloride ions --- TiO2 nanotubes --- g-C3N4 --- response surface methodology --- wastewater treatment --- phenol --- crude oil --- sonolysis --- sonophotocatalysis --- FT-ICR/MS --- Kendrick plot --- van Krevelen diagram --- water --- pollution --- remediation --- Au-TiO2 --- antibiotics --- emergent contaminants --- nanocatalyst --- photocatalysis --- GFN-xTB --- ibuprofen --- advanced oxidation process --- TiO2 --- active glass --- heterojunction --- charge separation --- chlorpyrifos --- photodegradation --- nanoparticles --- gold --- cyclodextrins --- perfluorooctanoic acid --- emerging contaminant --- defluorination --- platinum --- electro-oxidation --- strontium carbonate (SrCO3) --- solvothermal method --- visible light --- diethyl phthalate --- photoelectrochemical degradation --- persistent organic pollutants --- chloride ions --- TiO2 nanotubes --- g-C3N4 --- response surface methodology --- wastewater treatment --- phenol --- crude oil --- sonolysis --- sonophotocatalysis --- FT-ICR/MS --- Kendrick plot --- van Krevelen diagram --- water --- pollution --- remediation

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Water pollution from biorefractory pollutants and emerging contaminants is still a very relevant problem worldwide. Examples of these pollutants include disinfection by-products, pharmaceutical and personal care products, persistent organic chemicals, as well as their degradation products. The occurrence of these contaminants in water has raised increasing concern due to their accumulation and persistence in the environment and the threat they pose to the ecological system and human health. In this Special Issue, papers regarding the advancements in materials and processes for use in the electro- and photoelectrochemical removal of different pollutants from water are collected. The synthesis, characterization and application of materials for use in electrochemical or photoelectrochemical techniques are presented, as well as studies concerning catalytic processes and reaction kinetics.

Au-TiO2 --- antibiotics --- emergent contaminants --- nanocatalyst --- photocatalysis --- GFN-xTB --- ibuprofen --- advanced oxidation process --- TiO2 --- active glass --- heterojunction --- charge separation --- chlorpyrifos --- photodegradation --- nanoparticles --- gold --- cyclodextrins --- perfluorooctanoic acid --- emerging contaminant --- defluorination --- platinum --- electro-oxidation --- strontium carbonate (SrCO3) --- solvothermal method --- visible light --- n/a --- diethyl phthalate --- photoelectrochemical degradation --- persistent organic pollutants --- chloride ions --- TiO2 nanotubes --- g-C3N4 --- response surface methodology --- wastewater treatment --- phenol --- crude oil --- sonolysis --- sonophotocatalysis --- FT-ICR/MS --- Kendrick plot --- van Krevelen diagram --- water --- pollution --- remediation

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Semiconductor photocatalysts have attracted a great amount of multidiscipline research due to their high potential for solar-to-chemical-energy conversion applications, ranging from water and air purification to hydrogen and chemical fuel production. This unique diversity of photoinduced applications has spurred major research efforts on the rational design and development of photocatalytic materials with tailored structural, morphological, and optoelectronic properties in order to promote solar-light harvesting, easy photogenerated electron-hole recombination and the concomitant low quantum efficiency. This book presents a collection of original research articles on advanced photocatalytic materials, synthesized by novel fabrication approaches and/or innovative modifications that improve their performance in target photocatalytic applications such as water (cyanobacterial toxins, antibiotics, phenols, and dyes) and air (NOx and volatile organic compounds) pollutant degradation, hydrogen evolution, and hydrogen peroxide production by photoelectrochemical cells.

Technology: general issues --- anatase --- brookite --- C/N-TiO2 --- microcystin-LR --- photodegradation --- visible light --- TiO2 nanomaterials --- Au nanoparticles --- anodization --- photocatalytic degradation of antibiotics --- LC-MS/MS --- TiO2 --- photonic crystals --- graphene oxide nanocolloids --- reduced graphene oxide --- photocatalysis --- photocatalytic materials --- nanocomposites --- sulfate-modified BiVO4 --- methylene blue --- LED visible light --- photodecomposition --- anatase TiO2 nanocrystals --- high-energy facets --- photocatalytic activity --- photovoltaic performance --- photoactive cement --- TiO2/N --- NOx decomposition --- mechanical properties --- plasmonic photocatalysis --- silver-copper oxide --- VOCs remediation --- full-spectrum photoresponse --- carbon-doped titania --- carbon-modified titania --- graphene/titania --- vis-active photocatalyst --- antibacterial properties --- laser pyrolysis --- hydrogen peroxide --- CdS --- CdSe --- photoelectrocatalysis --- photocatalytic fuel cells --- photo fuel cells --- visible light activated titania --- heterojunction photocatalysts --- photonic crystal catalysts --- graphene-based photocatalysts --- water and air purification --- solar fuels