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Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered. About the Editors: Katja Dettmer-Wilde is Principal Investigator heading the mass spectrometry - metabolomics group at the Institute of Functional Genomics, University of Regensburg, Germany. She studied chemistry at the University of Leipzig and got her PhD with Werner Engewald working on the analysis of volatile organic compounds by GC-MS. Since her postdoctoral studies at the University of California Davis she has been focusing on hyphenated separation techniques in metabolomics. Werner Engewald is professor emeritus of the University of Leipzig, Germany. He is one of the leading gas chromatographers worldwide and has made substantial contributions towards the development of this technique. He regularly gives courses for GC users. He was awarded the Martin gold medal of the Chromatographic Society in 2002 and the Clemens-Winkler-Medal of the Division of Analytical Chemistry of the German Chemical Society in 2009. .
Fysicochemical separation methods --- Chemistry --- Toxicology --- Pharmacology. Therapy --- Environmental protection. Environmental technology --- MS GC (massaspectrometrie gaschromatografie) --- klinische chemie --- farmacologie --- genomics --- chemie --- multimedia --- toxicologie --- milieutechnologie --- chromatografie --- GC (gas chromatography) --- oplosmiddelen
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The text provides comprehensive coverage of basic topics in the field, such as stationary phases, packed columns and inlets, capillary columns and inlets, detectors, and qualitative and quantitative analysis. At the same time, the coverage also features key additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gas chromatography Along with these new and updated topics, the references, resources, and Web sites in Basic Gas Chromatography have been revised to reflect the state of the field. Concise and fundamental in its coverage, Basic Gas Chromatography, Second Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists.
Fysicochemical separation methods --- gas chromatography --- solvent --- MS GC (massaspectrometrie gaschromatografie) --- scheidingstechnieken --- GC (gas chromatography) --- Gas chromatography --- Analytische chemie --- Chromatografie; gaschromatografie --- Gas-liquid chromatography --- GLC (Chromatographic analysis) --- Vapor-phase chromatography --- Chromatographic analysis
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Understanding Mass Spectra: A Basic Approach, Second Edition combines coverage of the principles underlying mass spectral analysis with clear guidelines on how to apply them in a laboratory setting. Completely revised from the first edition, an updated and unified approach to mass spectral interpretation emphasizes the application of basic principles from undergraduate organic, analytical, and physical chemistry courses. A detailed overview of theory and instrumentation, this useful guide contains step-by-step descriptions of interpretative strategies and convenient lists and tables detailing the information needed to solve unknowns. Other features include real-world case studies and examples, skill-building problems with clearly explained answers, and easy-to-follow explanations of the important mathematical derivations.
Mass spectrometry. --- Physicochemistry --- Spectrometric and optical chemical analysis --- Fysicochemical separation methods --- Organic spectroscopy --- Organic chemistry --- organic chemistry --- spectrometry --- gas chromatography --- isotopes --- gamma ray spectrometry --- aromatic hydrocarbon --- massaspectrometrie --- MS GC (massaspectrometrie gaschromatografie) --- isotopen --- massaspectroscopie --- organische chemie --- massaspectra --- siliconen --- GC (gas chromatography) --- fysicochemie --- spectrometrie
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Select the Right Analytical Instruments to Optimize Scientific and Engineering Projects and Research The Handbook of Analytical Instruments offers scientists and engineers a complete guide to the principles and building blocks of today's high-tech instruments, so that they can select the right analytical tools to optimize their projects and research. This expert resource covers instrumentation basics and recent advances, such as biosensorsgamma spectrometers and visualization methods for electrophoresis. The book takes readers through flame photometers, radiochemical instruments, automated chemical analysis systems, blood gas analyzers, digital circuits, and much more. Filled with 100 detailed illustrations, the Handbook of Analytical Instruments fully explores: The integration of microcontrollers and personal computers, resulting in improved recording techniques and display systems Advances in spectrophotometry, leading to ever-decreasing sample size and multi-sample analytical techniques The latest electrochemical instruments\_with greater speed, accuracy, and automation Get Quick Access to Today's Most Powerful Analytical Instruments Fundamentals of Analytical Instruments Colorimeters and Spectrophotometers Infrared Spectrophotometers Flame Photometers Atomic Absorption Spectrophotometers Fluorimeters and Phosphorimeters Raman Spectrometers Photoacoustic and Photothermal Spectrometers Mass Spectrometers Nuclear Magnetic Resonance Spectrometers Electron Spin Resonance Spectrometers Electron and Ion Spectroscopy Radiochemical Instruments X-Ray Spectrometers Automated Chemical Analysis Systems Gas Chromatographs Liquid Chromatographs Thermo-Analytical Instruments Electrophoresis Apparatus and Densitometers Electrochemical Instruments pH Meters and Ion Analyzers Blood Gas Analyzers Industrial Gas Analyzers Environmental Pollution Monitoring Instruments Electronic Devices and Circuits Digital Circuits Computer-Based Analytical Instruments
Nuclear physics --- Electrochemistry --- Spectrometric and optical chemical analysis --- Fysicochemical separation methods --- Analytical chemistry --- colorimetry --- nuclear physics --- infrared spectroscopy --- densitometers --- spectrometry --- spectrophotometry --- gas chromatography --- photoacoustic spectroscopy --- mass spectrometry --- electrochemistry --- Raman spectroscopy --- colorimetrische analyse --- massaspectrometrie --- MS GC (massaspectrometrie gaschromatografie) --- IR spectroscopie --- FAS (fotoakoestische spectroscopie) --- magnetische resonantie spectrometrie --- LC MS (liquid chromatography massspectrometry) --- analyse (chemie) --- LC GC (liquid chromatography gas chromatography) --- GC (gas chromatography) --- elektrochemie --- spectrometrie --- spectrofotometrie
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This highly successful textbook, acclaimed for its comprehensiveness, accuracy, and its many excellent illustrations and photographs now comes in its second edition. Completely revised and substantially extended it offers: New chapter on **Tandem Mass Spectrometry** covering instrumentation, methods for ion activation (CID, ECD, ETD, IRMPD), and applications New chapter on **Ambient Mass Spectrometry** (DART, DESI, and more) New chapter on **Inorganic Mass Spectrometry** including element speciation and imaging **Learning Objectives** for all chapters **Advanced Instrumentation** such as orbitraps, linear ion traps, tandem TOFs, FT-ICR and the highly variable hybrid instruments Updated **Problems and Solutions website** (www.ms-textbook.com) ***Jürgen H. Gross*** provides in-depth explanations of concepts, methods, and techniques. Students and professionals alike are guided step-by-step from the basics to the successful application of mass spectrometry. Starting from the very principles of gas-phase ion chemistry, isotopic composition, and accurate mass, ***Jürgen H. Gross*** leads through the design of all types of mass analyzers and ionization methods to mass spectral interpretation and coupling techniques. His book offers a balanced mixture of practice-oriented information and theoretical background supported by a wealth of references. Keywords Analytical Chemistry - CID, IRMPD, ECD, ETD - Chemical Ionization - DART, DESI, DAPCI - Electron Ionization - Electrospray Ionization - Fast Atom Bombardment - Field Desorption - Field Ionization - Inorganic Mass Spectrometry - Isotope Ratio - LIFDI - MALDI - Mass Spectrometry - TOF/TOF - Tandem Mass Spectrometry - Textbook
spectrometrie --- fysicochemie --- gas chromatography --- organic chemistry --- Organic chemistry --- MS GC (massaspectrometrie gaschromatografie) --- Spectrometric and optical chemical analysis --- massaspectrometrie --- isotopes --- organische chemie --- isotopen --- Physicochemistry --- spectrometry --- Fysicochemical separation methods --- GC (gaschromatografie) --- Organic spectroscopy --- Spectrométrie --- Spectrometry --- methods --- Analytische chemie --- Spectrometrie --- Analytical biochemistry. --- Chemistry. --- Chemistry, Physical organic. --- Environmental toxicology. --- Polymers. --- Proteomics. --- Mass spectrometry --- Ionization --- Analytical Chemistry --- Chemistry --- Physical Sciences & Mathematics --- Monograph --- GC (gas chromatography) --- Mass spectra --- Mass spectrograph --- Mass spectroscopy --- Mass spectrum analysis --- Mass (Physics) --- Nuclear spectroscopy --- Spectrum analysis --- Scission (Chemistry) --- Analytical chemistry. --- Ecotoxicology. --- Physical chemistry. --- Polymers . --- Physical measurements. --- Measurement . --- Analytical Chemistry. --- Physical Chemistry. --- Polymer Sciences. --- Measurement Science and Instrumentation. --- Measuring --- Mensuration --- Mathematics --- Technology --- Metrology --- Physical measurements --- Measurements, Physical --- Mathematical physics --- Measurement --- Molecular biology --- Proteins --- Polymere --- Polymeride --- Polymers and polymerization --- Macromolecules --- Chemistry, Theoretical --- Physical chemistry --- Theoretical chemistry --- Ecotoxicology --- Pollutants --- Pollution --- Environmental health --- Toxicology --- Analysis, Chemical --- Analytic chemistry --- Chemical analysis --- Chemistry, Analytic
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