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Methods for the calibration and use of germanium spectrometers for the measurement of gamma-ray energies and emission rates over the energy range from 59 keV to approximately 3000 keV and for the calculation of source activities from these measurements are established. Minimum requirements for automated peak finding are stated. Methods for measuring the full-energy peak efficiency with calibrated sources are given. Performance tests that ascertain the proper functioning of the Ge spectrometer and evaluate the limitations of the algorithms used for locating and fitting single and multiple peaks are described. Methods for the measurement of and the correction for pulse pileup are suggested. Techniques are recommended for the inspection of spectral-analysis results for large errors resulting from summing of cascade gamma rays in the detector. Suggestions are provided for the establishment of data libraries for radionuclide identification, decay corrections, and the conversion of gamma-ray rates to decay rates.

Germanium diodes --- Standards.

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Methods are established for performance testing, calibration, and use of sodium iodide detector systems for the measurement of gamma-ray emission rates of radionuclides, assay for radioactivity, and the determination of gamma-ray energies. Both energy calibration and efficiency calibration are covered. Three techniques are considered: total spectrum counting, which employs a system that counts all events above a low-energy threshold; single-channel analyzer counting, which employs a system with a counting window that establishes upper and lower energy boundaries; and multichannel analyzer counting, which employs a system utilizing multiple counting windows.

Germanium diodes --- Gamma rays --- Standards. --- Measurement

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Germanium diodes. --- Semiconductor doping. --- Infrared detectors.

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Gamma rays --- Germanium diodes --- Measurement --- Standards. --- Standards.