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Dissertation
Hydration force and phase transitions of phospholipids

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Dissertation
Innovative NDT techniques for aircraft maintenance : Acoustic fuel tank monitoring and thermal fuselage inspections
Authors: --- --- ---
Year: 2022 Publisher: Leuven KU Leuven. Faculty of Engineering Science

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In this work, non-invasive measurement methods are used to solve problems in daily aircraft maintenance. The measurement methods used are based on the Acoustic Emission Technique, Infrared Thermography and Laser Doppler Vibrometry. The procedures and analysis methods are not entirely new, but they can, however, be considered new in the context of the described aircraft maintenance work. Therefore, it is possible to speak of innovative non-invasive measurement methods in aircraft maintenance. Two explicit questions that arise directly from aircraft maintenance in daily operations are addressed. A well-known problem in civil aviation is water accumulation in fuel tanks, which aircraft operators face daily. This water accumulation and the resulting ice that forms during flight can lead to costly and sometimes very dangerous situations. Therefore, efforts are underway to develop a reliable detection system to determine the remaining amount of accumulated ice after flight and during recovery operations. By using such a technology, it would be possible to increase the safety and efficiency of aircraft operations in this highly competitive market. This PhD manuscript discusses the use of the Acoustic Emission Technique to reliably and non-invasively monitor the melting of ice in fuel tanks. This technique is based in principle on the fact that a phase transition is often accompanied by stress relaxation, which can be used to monitor the process. Therefore, the melting of ice can essentially be monitored with AE without directly accessing the ice. The findings presented in this work can potentially lead to new technologies for ice detection, especially in remote areas that are not easily accessible with other techniques. The second application of novel inspection methods based on non-invasive measurement methods concerns the inspection of fasteners in aluminum joints. In the aerospace industry, such inspections are time-consuming and costly, but mandatory. Until today, manual methods use mainly the naked eye and do not allow the tracking of damaging behavior over time or objective comparison between different inspections. A digital inspection procedure addresses both shortcomings while leading to a significant reduction in inspection time. The aim is to compare three inspection methods based on measurements on a serviceable aircraft component. An essential part of this is the development of a new digital and automated inspection method based on in-plane heatwave thermography, which is based on the analysis of thermal disturbances caused by irregularities in the plate-like structure. Simultaneously, measurements are made using ultrasonic lock-in thermography and a scanning laser Doppler vibrometer. Benchmarking of all three methods is performed on an operational aircraft fuselage panel. The data presented confirm the feasibility of detecting damage and qualifying countersunk rivets and screws in aluminum fuselage panels using the methods discussed.

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Dissertation
Dedicated Solutions for Structural Health Monitoring of Aircraft Components

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Aircraft structures, like any other mechanical structure, are subjected to various external factors that influence their lifetime. Mechanicalnbsp;and the environment are only some of the factors that can degrade the structure of aircraft components. Monitoring of these degradations by regular inspections or automated data recording is vital for the structural health of the critical components of an aircraft. This research proposes a number of dedicated solutions for structural health monitoring (SHM) of aircraft components helping the detection of structural degradation.The dedicated solutions for SHM presented in this study include the following; 1. Flat coil sensors inspired by eddy current technology, 2. Electrical crack gauges for crack monitoring, 3. Optical fibres used for impact detection on composite materials, 4. SHM using ultrasonic Lamb waves testing with pseudo defects for signal validation as well as 5. Percolation sensors used for the detection of corrosion liquids in confined parts. The testing systems are applied in aircraft components made of aluminium, maraging steel and monolithic and sandwich carbon fibre reinforced polymers (CFRP).The flat coil sensors are glued on aluminium 2024-T3 plates and are able to detect fatigue cracks in critical areas. The critical area is a hole in the middle of the plate which is a stress concentrator. The sensors are based on eddy currents that are induced into the material. Structural discontinuities under the surface of the material alter the electromagnetic properties of the coil showing an impedance change relevant to the crack size. It was found that a 2% increase of the relative difference of impedance corresponds to a crack size of 10 mm within the materials investigated.The electrical crack gauges are glued on aluminium 2024-T3 plates and on an Airbus A320 slat-track. The crack gauges are made of an electrically conductive component and are connected to an ohmmeter. It was found that by exposing the plates to fatigue, simulating flight conditions, the electrical gauges,nbsp;to the loss of their electrical conductivity, can reveal the crack growth.The optical fibres are attached to monolithic and sandwich CFRC of floor panels and in a EC 135 tailboom. Lamb waves generated from a forced impact arrive at the optical fibres leading to an anisotropic refractive index, called birefringence. The pressure levels from the incident elastic waves result in a change of intensity due to a polarization rotation of the light propagating through the optical fibre. It was found that optical fibres offer some advantages compared to conventional piezoelectric transducers and the differentiation of the signal between input and output can reveal information on the impact force and on delaminations presence.The pseudo defects are used for the validation of ultrasonic Lamb waves testing. It is well known that piezoelectric transducers can be used to excite and receive Lamb waves. These elastic waves can propagate through thin plates. Pseudo defects of different size and shape are placed on the plate in various angles and positions and the acoustic response with and without defect is compared and validated for SHM purposes. It wasnbsp;that a correlation of the signals of the real defects and the pseudo defects is feasible and it can lead to a mapping for the probability of detection (POD) of real defects at different positions.The percolation sensors are used in confined spaces in order to detect aqueous liquids or high humidity levels that can cause corrosion. The sensors are made of an organo-ceramic composite that consists of a conductive Titanium Carbonitride (TiCN) powder and Polyvinyl Alcohol (PVA). The concept of this sensor relies on the collapse of the percolation conductivity of the sensor due to swelling from aqueous absorption. This results in a sudden change in the electrical resistance of the conducting part. The sensor was validated concerning its temperature behaviour and its exposure in different levels of humidity with the aid of 10 salt solutions. It was found that the sensors can be used successfully, they were embedded now into three operational airplanes and due to their innovativenbsp;they have been patented.The tests were conducted in the laboratories of the Department of Materials Engineering (MTM) and the Department of Physics and Astronomy (FYS) of KU Leuven, Belgium as well as in the German Aerospace Centre (DLR) in Braunschweig, Germany.nbsp;aircraft components were obtained from ASCO Industries, Belgium and Eurocopter (Airbus Helicopters), France. The research conducted for this PhD thesis was a part of the Aircraft Integrated Structural Health Assessment (AISHA II) European project from the 7th Framework Programme of the European Commission.

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Dissertation
Harmful liquids and vapours in space structures - Detection and Prevention
Authors: --- --- ---
Year: 2021 Publisher: Leuven KU Leuven. Faculteit Wetenschappen

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During the history of the space sector, a tremendous amount of money has been involved. The best known and biggest agencies such as NASA and ESA invest huge sums of money to reach space with their missions. In the past, this was the only way, but nowadays smaller, lower budget companies with a single business man at the top, think of Elon Musk, are emerging. Their focus is to find a cheaper, and even more importantly, a more sustainable way for space travel. This changed the industry big time and re-usability became a must. A second evolution in the space sector is the increase of mission duration. Astronauts are preparing for long duration missions to the moon and Mars, where resupplying becomes increasingly difficult and a process of a long time. Therefore, it becomes more and more important to reduce the need of redundant parts and to increase the lifetime of space structures. This can be, although partially, achieved by researching and tackling issues regarding contamination. The term contamination includes all unwanted matter affecting or degrading the performance and/or lifetime of the spacecraft. It can result from manufacture on Earth, through deposition on surfaces or due to a process called outgassing, where gas is released that was previously contained in materials. Another source is the human crew, who breathe and sweat, but also for whom a habitable environment with a sufficient humidity level has to be provided. These contaminants can induce a whole range of issues, from the growth of dangerous microorganisms to the degradation of structural materials and subsystems. They might actually endanger the whole mission. A lot of preventive measures are already in place to avoid contamination as much as possible, e.g. strict clean room environments on Earth, criteria for material selection, active air filtering onboard etc. However, it seems that, to some extend, contamination might be unavoidable. Therefore, in addition to an elaborated description of the situation in nowadays space operations, the proposition in this thesis is to construct a tool kit with ready to go sensors that astronauts can implement themselves, named the “space sensor kit”. This way they can perform research on the different types of contamination, but they can also implement them in areas they think as crucial. Contaminant sensitive areas in spacecraft can change throughout its lifetime and crew members will have the best knowledge of the structure and will be most capable of making well considered choices. The space sensor kit would include three versatile sensors based on different physical phenomena, with their own specific advantages, that can be implemented during operations in space.

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Dissertation
Time Domain Reflectometry (TDR) for detecting leakage damage in large engineering structures

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During previous research, percolation-based PVA/TiCN and silicone/graphite sensors have been designed and tested at the Department of Materials Engineering at KU Leuven for the detection of water and kerosene leakages. An approximately exponential increase of the DC resistance at the lyotropic percolation threshold allowed a fuse-like detection of the leakage. However, the localisation of the leakage along the sensor length was not possible and hence, the feasibility of a combination with the simple, low-cost and fast nondestructive Time domain reflectometry (TDR) technique was studied within this thesis to localise the leakage spot. Detection and localisation of multiple leakage spots along both sensors was possible. The differential evolution of the sensor’s TDR voltage was monitored during each experiment and compared to the dry sensor. Leakage spot sizes of 10 and 4 cm were clearly detected for respectively the water and kerosene sensor. The proposed sigmoidal fitting method of the differential voltage allowed accurate localisation of the leakage spots. When two leakage spots were simultaneously applied at the sensor, the differential peak for each leakage spot could be distinguished and localised. A lumped circuit model based on the dimensional and electromagnetic properties of the sensor’s constituting layers accurately predicted the reflection of the applied voltage wave at both the sensor entrance and the applied leakage spot. The observed negative differential TDR peak for a water leakage was assumed to be caused by a local increase in the permittivity of PVA. For the kerosene sensor, a positive differential TDR peak was seen, which was attributed to the fuse-like increase of the sensor’s resistance due to a kerosene-induced disruption of the percolative graphite network. TDR was concluded to offer a sensitive detection and accurate localisation solution for leakage monitoring in large engineering structures like fuselages of aircrafts and pipelines. Its combination with DC resistance monitoring allows the lay-out of a distributed sensor network in these structures for low-cost, flexible and continuous Structural Health Monitoring. The sensor’s low materials cost of approximately € 1-2/m makes it clearly advantageous over the currently available commercial leakage sensors.

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Dissertation
Optimizing acoustic emission-based detection technology of sessile ice droplets for aerospace and other engineering applications
Authors: --- --- --- ---
Year: 2022 Publisher: Leuven KU Leuven. Faculteit Ingenieurswetenschappen

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The aim of this investigation is to determine whether the acoustic response of a melting ice droplet can be reliably monitored in a reproducible fashion for different icing scenarios. The end-goal is to optimize an acoustic emission (AE)-based ice sensing technology that can detect ice accumulation inside an aircraft fuel tank or on the surface of an aircraft wing or a wind turbine blade. This was achieved by acoustically monitoring the melting of ice droplets adhering to an aluminium substrate and evaluating the influence of a variety of parameters. When no influencing factors were implemented, a strong variability in the acoustic response was observed. This was most likely the result of frost acoustic signals. In addition, by testing the influence of droplet size and ice porosity, it was shown that larger droplets would not necessarily lead to more AE because they had more air inclusions that could scatter sound waves. Similarly, porous ice had a much less intensive acoustic response than non-porous ice. In addition, impurities arising from kerosene will decrease the acoustic intensity. This could be due to the presence of supercooled liquid domains within the ice droplet that decrease the amount of potential AE sources. Finally, purposely accelerating freezing by playing on the surface temperature will not affect the resulting acoustic behaviour of a melting droplet. From this study, a first set of boundary conditions to a repeatable and reliable detectability was set but further spectral, thermodynamical and microscopical analysis are required for a more in-depth understanding of those boundary conditions. Repeating these experiments with much larger sample sizes for more representative results is of high importance.

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Dissertation
Detection of cracks in tubes by mode conversion assessment of laser generated guided waves
Authors: --- --- --- ---
Year: 2019 Publisher: Leuven KU Leuven. Faculteit Ingenieurswetenschappen

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Crack detection of cylindrical components such as rods, tubes, etc. has always been of great significance in structural health monitoring (SHM) research. Researchers have already tackled a variety of advanced non-destructive testing (NDT) techniques to investigate crack generation and growth in test samples. As laser technology is progressing, photoacoustic generation and optical detection of guided acoustic waves that are sensitive to defects has emerged as a promising approach for NDT and SHM. The focus of this thesis lies on the exploration of the use of laser ultrasonic generation and laser Doppler vibrometry detection for crack detection in cylindrical components. Starting from fundamental wave propagation equations and the theory of Lamb wave mode propagation through an intact plate, simulations are made for mode conversion by a crack of a certain depth normal to the plate surface, using a modal decomposition approach in combination with singular value decomposition. The method is based on searching for the amplitudes of modes, which, summed up together, satisfy boundary conditions for displacement and stress in the plane of the defect. The quality of boundary condition fulfilment as well as the degree energy conservation are used as a validation of the accuracy of the method. An experimental set-up has been built to detect the acoustic waves through brass rods and copper tubes in three states: intact, with an open crack and with a closed crack. These measurements are found to be qualitatively consistent with predictions obtained by numerical calculations, both in terms of acoustic wave dispersion and degree of mode conversion. The results confirm that, by exploiting the influence of the state of opening/closing of a defect on mode conversion, detection of correlation between the dynamics of stress applied on a component and of the degree of mode conversion may be a viable method for defect detection.

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Dissertation
Selection, design and characterisation of a composite material for low frequency underwater acoustic damping

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Underwater sea drones are used for both mapping the seabed and in the search of foreign objects (ships or plane wrecks) on the seabed. Current drone sonars receive unwanted surface reflected sound waves, interfering with acoustic waves that contain useful information. With the current sonars, the unwanted waves are programmed out, although resulting in information loss. The accuracy of the sonars can thus be improved by placing an acoustic damping material on top of the sonar, resulting in a cleaner input. These sonars function at low frequencies in order to search the sub-seabed, while most known underwater damping materials are only capable dampers in higher frequency ranges. Therefore, the scope of this thesis is to design a material that functions in the low frequency range of 0.5 to 10 kHz, damping up to 90 % of underwater acoustic waves. Based on the literature, a polyurethane (PU) matrix mixed with 1 vol% carbon fibre (CF) inclusions with a total thickness of 2-3 cm was selected. This composite was characterized via modelling, showing that adding CF to a pure PU matrix resulted in enhanced sound attenuation. A decrease in PU porosity from 5 % to 1 % air porosity was modelled to increase acoustic performance under high hydrostatic pressure, as attenuation increased from 6 to 14 dB at 300 m (5 kHz). In addition to modelling, experimental characterisation was conducted using two water based test set-ups. Adding CF via shear mixing, to a pure PU matrix, in a sample of 3 cm thickness increased the attenuation by 8.5 dB at 1 kHz. Attenuation was optimal when the CFs were dispersed via shear mixing, resulting in CF clusters, potentially hindering the acoustic wave propagation, and when the PU components were degassed. The achieved dispersion of the CF was characterized, both micro- and macroscopically, with the macroscopic dispersion of a sonicated sample showing that an area of 97.5 % contained CF, while in the shear mixed sample the dispersion was less homogeneous at 83 %. A CF of type 'IM' with a higher Young's modulus and aspect ratio was found to result in an attenuation increase from 4.5 dB to 8.5 dB (1 kHz). To conclude, a degassed PU matrix with 1 vol% CF inclusions of type 'IM' randomly dispersed using only shear mixing was found to significantly increase acoustic low frequency attenuation, which can be used to successfully improve the accuracy of future underwater sonar drones.

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Dissertation
Durability of post-tensioning systems for concrete bridges in view of moisture ingress

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This master’s thesis discusses durability issues of post-tensioning systems for concrete bridges with a focus on moisture ingress. It consists of two parts: an extensive literature study and a smaller experimental part. The literature study first discusses different post-tensioning systems and their equip- ment needed. The two most relevant systems for bridge applications are the internal, bonded post-tensioning and the external (bonded and unbonded) systems. Internal, bonded systems are most widely used and grout issues play a major role in those systems. The starting point in assessing the various durability issues lies with nine different case studies. These cases range from bridge failures in the UK and Italy, to repairs of deficient grout, and addition external post-tensioning. Subsequently, the durability issues are further explained and discussed, going from the cause and the consequences to the mains to repair, remediate and prevent those issues from happen- ing in the future. It became clear that chloride-induced corrosion is the main cause of durability problems, with stress corrosion cracking possibly increasing the speed of deterioration. The most effective way to prevent these corrosion issues is by making sure no water (with possible chlorides) can reach the prestressing steel. This is done by providing multiple independent protective layers and rethinking the placement of anchorages. Inspection and monitoring techniques are necessary to detect voids, deficient grout, damaged tendons and corrosion. Various methods are discussed, taking into account the applicability to post-tensioning systems. It became apparent that every technique (non-, semi-, or destructive) has its application field, but varying results are possible and appropriate expertise is needed to interpret the measurements. The second part of this master’s thesis acts as a proof of concept whether percolation sensors have the potential to be applicable for monitoring moisture ingress within a post-tensioning duct. This would be useful because such an environment could lead to corrosion of prestressing steel. The resistance over the used TiCN-PVA percolation sensors shows an increase of multiple orders of magnitude when 80% relative humidity is reached (an “on”/“off” sensor). However, after wetting of the samples during the experiment, the resistance over the sensors decreased instead of increasing. In addition to other behaviour, this led to believe that the (DC) resistance over the grout itself was monitored. The sensor contacts were not isolated from their surroundings, making the latter possible. Further research is thus necessary before providing a clear conclusion regarding this research question.

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Dissertation
Interfacial adhesion in Aramid reinforced thermoplastic composites: Determination of work of adhesion at high temperatures

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In a world where efficiency and therefore weight reduction are becoming more important, composite materials can offer a solution. Fibre reinforced composites are materials that consist of at least two different materials, one fibre phase and a matrix phase. Besides studying the properties of these individual materials it is important to study how those materials interact with each other. This thesis starts with determining the compatibility of different fibre matrix combinations at room temperature. A frequently used method to study the compatibility is based on the surface energy components. These are determined by contact angle measurements of fibres and polymer films with different test liquids at room temperature. One important parameter to judge the compatibility is the work of adhesion. At room temperature this one is calculated based on the acid-base theory. The second part of this thesis tried to develop a new method to determine the work of adhesion of a system. Instead of calculating the work of adhesion at room temperature this method aimed to determine it at high temperature. This method was based on determining the contact angle between one fibre and a droplet. It was easier to accurately measure the inflection angle of the droplet then measure the contact angle directly. Therefore this method measured the inflection angle at high temperature. This method delivered some unexpected results. Even in an inert environment the droplet volume of polypropylene droplet was decreasing. This influenced the contact angle measurements. When the volume decreased the contact angle measured was the receding contact angle and not the advancing since the embedded length was decreasing. To finalise this thesis tried to measure the interfacial shear strength(IFSS) using a microdroplet pull out test equipped with acoustic emission. Even though the setup was similar to previous research using this technique this method didn’t have useable results. The IFSS was calculate using the shear-lag model as well as the ‘alternative’ Zhandarov model. The results from the Zhandarov model suggest that the interphase already had some failure before testing since they were not constant for larger embedded lengths.

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