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This is the first general textbook on experimental design and optimization in organic synthesis. The book presents a unified methodology for carrying out systematic studies when the objective is to develop efficient and optimum synthetic methods. Strategies are included both for exploring the experimental conditions and for systematic studies of entire reaction systems (substrates, reagent(s) and solvents). The methodology is based on multivariate statistical techniques. The following topics are treated in depth: classical two-level designs for screening experiments, gradient method
Chemical reaction, Conditions and laws of. --- Organic compounds --- Synthesis. --- Chemistry, Organic --- Chemistry, Synthetic organic --- Organic synthesis (Chemistry) --- Synthetic organic chemistry --- Conditions and laws of chemical reaction --- Reaction, Conditions and laws of (Chemistry) --- Chemistry, Physical and theoretical --- Physical laws --- Synthesis --- Composés organiques --- Synthèse
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Organic compounds --- Composés organiques --- Synthesis --- Synthèse
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This is the first general textbook on experimental design and optimization in organic synthesis. The book presents a unified methodology for carrying out systematic studies when the objective is to develop efficient and optimum synthetic methods. Strategies are included both for exploring the experimental conditions and for systematic studies of entire reaction systems (substrates, reagent(s) and solvents). The methodology is based on multivariate statistical techniques. The following topics are treated in depth: classical two-level designs for screening experiments, gradient methods (steepest ascent, simplex methods) as well as response surface techniques for optimization, principal components analysis and PLS modelling. The book is intended as a hands-on text for chemists and engineers engaged in developing synthetic methods in industrial research, e.g. in fine chemicals and pharmaceuticals production, as well as for advanced undergraduate students, graduate students, and researchers in an academic environment.
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Revised, and updated Design and Optimization in Organic Synthesis presents strategies to explore experimental conditions and methodologies for systematic studies of entire reaction systems (substrates, reagent(s), catalyst(s), and solvents). Chemical phenomena are not usually the result of a single factor and this book describes how statistically designed methods can be used to analyse and evaluate synthetic procedures. The methodology is based on multivariate statistical techniques. The accompanying CD contains data tables and programmes. This book is essential reading for anyone worki
Organic compounds --- 547.057 --- Chemistry, Organic --- Chemistry, Synthetic organic --- Organic synthesis (Chemistry) --- Synthetic organic chemistry --- Synthesis --- Organic synthesis --- Chemistry, Organic. --- Organic chemistry --- Chemistry --- Synthesis.
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Revised, and updated Design and Optimization in Organic Synthesis presents strategies to explore experimental conditions and methodologies for systematic studies of entire reaction systems (substrates, reagent(s), catalyst(s), and solvents). Chemical phenomena are not usually the result of a single factor and this book describes how statistically designed methods can be used to analyse and evaluate synthetic procedures. The methodology is based on multivariate statistical techniques. The accompanying CD contains data tables and programmes. This book is essential reading for anyone working in process design and development in fine chemicals or the pharmaceutical industry, and is suitable for those with no experience in the field. * Contains recalculated models and redrawn figures, as well as new chapters on for example, the design of combinatorial libraries * Presents strategies to explore experimental conditions and methodologies * Enables the analysis and prediction of the best synthetic procedures.
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Speech/language and music are the two main forms of systematic human communication using acoustic signals. This implies that there are interesting and thought-provoking parallels between these areas, which may contribute towards our understanding of the processing and perception of auditory signals. This book reviews the relevant research fields, and includes speech and music examples on CD to help the reader to appreciate the sound characteristics discussed. Areas covered are: descriptions of music and language; speech and music performance; voice and instruments; cognition and perception; neurophysiology; combining speech and music.
Cognitive neuroscience --- Music --- Speech --- Neurosciences cognitives --- Musique --- Parole --- Congresses --- Physiological aspects --- Congrès --- Aspect physiologique --- Congrès --- Human physiology. --- Music. --- Human Physiology. --- Art music --- Art music, Western --- Classical music --- Musical compositions --- Musical works --- Serious music --- Western art music --- Western music (Western countries) --- Human biology --- Medical sciences --- Physiology --- Human body
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Speech perception --- Acoustic nerve --- Hearing --- Auditory pathways --- Auditory perception --- Speech perception --- Perception de la parole --- Nerf vestibulocochléaire --- Audition (Physiologie) --- Voies auditives --- Perception auditive --- Perception de la parole --- Physiology --- Congresses --- Physiology --- Congresses --- Physiology --- Congresses --- Congresses --- Congresses --- Congresses --- Physiologie --- Congrès --- Physiologie --- Congrès --- Congrès --- Congrès --- Congrès --- Congrès
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