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The importance of chiral interactions for both preparative and analytical separations, particularly for pharmaceutical applications, is underlined by numerous publications in this field. Here, for the first time, a team of experienced analysts from industry and academe presents a comprehensive review of the various mechanisms that result in enantiomer separations. A better understanding of these processes is crucial for setting as well as improving chiral separation procedures and also for developing new applications. The coverage in this book includes a range of separation methods, such as gas, liquid, or countercurrent chromatography, and capillary electrophoresis. The special case of chiral ionic liquids is examined in detail. Most modern chiral selectors are discussed, including derivatized polysaccharide- and cyclodextrin-based selectors, along with a newly introduced class of carbohydrates: the cyclofructose selectors. This publication will be required reading not only for research and development departments in the pharmaceutical and cosmetic industries, but also for researchers in toxicology, environmental monitoring, and food research.

Chirality. --- Enantiomers -- Separation. --- Liquid chromatography. --- Molecular recognition --- Enantiomers --- Human Anatomy & Physiology --- Chemistry --- Health & Biological Sciences --- Physical Sciences & Mathematics --- Animal Biochemistry --- Analytical Chemistry --- Biotechnology --- Enantiomers. --- Chromatographic analysis. --- Analysis, Chromatographic --- Chromatography --- Antipodes, Optical --- Enantiomorphs --- Isomers, Mirror-image --- Mirror-image isomers --- Optical antipodes --- Chemistry. --- Pharmacy. --- Pharmacology. --- Chromatography. --- Food --- Pharmacology/Toxicology. --- Food Science. --- Environmental Monitoring/Analysis. --- Biotechnology. --- Chemistry, Analytic --- Phase partition --- Optical isomers --- Chirality --- Stereochemistry --- Symmetry (Physics) --- Toxicology. --- Food science. --- Monitoring/Environmental Analysis. --- Science --- Chemicals --- Medicine --- Pharmacology --- Poisoning --- Poisons --- Drugs --- Materia medica --- Toxicology --- Analytical chemistry --- Food—Biotechnology. --- Environmental monitoring. --- Biomonitoring (Ecology) --- Ecological monitoring --- Environmental quality --- Monitoring, Environmental --- Applied ecology --- Environmental engineering --- Pollution --- Drug effects --- Medical pharmacology --- Medical sciences --- Chemotherapy --- Pharmacy --- Measurement --- Monitoring --- Physiological effect

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The importance of chiral interactions for both preparative and analytical separations, particularly for pharmaceutical applications, is underlined by numerous publications in this field. Here, for the first time, a team of experienced analysts from industry and academe presents a comprehensive review of the various mechanisms that result in enantiomer separations. A better understanding of these processes is crucial for setting as well as improving chiral separation procedures and also for developing new applications. The coverage in this book includes a range of separation methods, such as gas, liquid, or countercurrent chromatography, and capillary electrophoresis. The special case of chiral ionic liquids is examined in detail. Most modern chiral selectors are discussed, including derivatized polysaccharide- and cyclodextrin-based selectors, along with a newly introduced class of carbohydrates: the cyclofructose selectors. This publication will be required reading not only for research and development departments in the pharmaceutical and cosmetic industries, but also for researchers in toxicology, environmental monitoring, and food research.

Nature protection --- Measuring methods in physics --- Fysicochemical separation methods --- History of human medicine --- Nutritionary hygiene. Diet --- Pharmacology. Therapy --- Environmental protection. Environmental technology --- Food science and technology --- monitoring --- voedingstechnologie --- farmacologie --- toxicologie --- voedingsleer --- electrophoresis --- milieutechnologie --- milieubeheer --- LC (liquid chromatography) --- chromatografie --- milieuanalyse

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1 Gas Chromatography: Theory and Definitions, Retention and Thermodynamics, and Selectivity 775 
Glenn E. Spangler 

2 Basic Overview on Gas Chromatography Injectors 807 
Md. Musfiqur Rahman, A.M. Abd El-Aty, and Jae-Han Shim 

3 Basic Overview on Gas Chromatography Columns 823 
Md. Musfiqur Rahman, A.M. Abd El-Aty, Jeong-Heui Choi, Ho-Chul Shin, Sung Chul Shin, and Jae-Han Shim 

4 Overview of Detectors in Gas Chromatography 835 
Md. Musfiqur Rahman, A.M. Abd El-Aty, and Jae-Han Shim 

5 Current Use of Gas Chromatography and Applications 849 
Walter Vetter 

6 Gas Chromatography with Mass Spectrometry (GC-MS) 883 
Walter Vetter 

7 Chiral GC 927 
Volker Schurig 

8 New Essential Events in Modern Applications of Inverse Gas Chromatography 979 
Adam Voelkel, Henryk Grajek, Beata Strzemiecka, and Katarzyna Adamska 

9 Chip-Based Gas Chromatography 999 
Hamza Shakeel and Masoud Agah 

10 Portable Gas Chromatography 1021 
Philip A. Smith 

11 Packed Column Sub- and Supercritical Fluid Chromatography 1051 
Caroline West, Syame Khater, and Eric Lesellier 

12 Instrumentation for Sub- and Supercritical Fluid Chromatography 1075 
Taghi Khayamian, Ali Daneshfar, and Hassan Ghaziaskar 

Index to Volume 3 I1-I18


Analytical chemistry --- liquid chromatography --- analytische chemie --- gas chromatography --- Fysicochemical separation methods --- chromatografie