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Nuclear Magnetic Resonance (NMR) is based on the fact that certain nuclei exhibit a magnetic moment, oriented by a magnetic field, and absorb characteristic frequencies in the radiofrequency part of the spectrum. NMR is now a leading technique and a powerful tool for the investigation of the structure and interaction of molecules. The present Landolt-Börnstein volume III/35 "Nuclear Magnetic Resonance (NMR) Data" is therefore of major interest to all scientists and engineers who use NMR to study the structure and the binding of molecules. Volume III/35 "NMR-Data" is divided into several subvolumes and parts. Subvolume III/35A contains the nuclei B-11 and P-31, subvolume III/35B contains the nuclei F-19 and N-15, subvolume III/35C contains the nucleus H-1, subvolume III/35D contains the nucleus C-13, subvolume III/35E contains the nucleus O-17, and subvolume III/35G contains the nucleus Se-77. More nuclei are planned for future volumes.
Physics. --- Physics, general. --- Solid State Physics. --- Spectroscopy and Microscopy.
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The reader is provided with information about methods of calibration of light sources and photodetectors as well as responsiveness of spectral instruments ranging from near infrared to vacuum UV spectral, 1200 – 100 nm, and radiation intensities of up to several quanta per second in absolute and arbitrary units. The author describes for the first time original methods of measurements they created and draws upon over 40 years of experience in working with light sources and detectors to provide accurate and precise measurements. This book is the first to cover these aspects of radiometry and is divided into seven chapters that examine information about terminology, units, light sources and detectors, methods, including author’s original ones, of absolute calibration of detectors, spectral instruments responsiveness, absolute measurements of radiation intensity of photoprocesses, and original methods of their study. Of interest to researchers measuring; luminescence spectra, light intensities from IR to vacuum UV, spectral range in wide-light intensity ranges, calibrate light sources and detectors, absolute or relative quantum yields of photoprocess determination.
Optical radiometry -- Instruments. --- Radiation -- Experiments. --- Radiation -- Measurement. --- Radiation --- Chemistry, Analytic --- Chemistry --- Physical Sciences & Mathematics --- Analytical Chemistry --- Measurement --- Experiments --- Measurement. --- Experiments. --- Chemistry. --- Spectroscopy. --- Microscopy. --- Materials science. --- Spectroscopy/Spectrometry. --- Spectroscopy and Microscopy. --- Characterization and Evaluation of Materials. --- Biological Microscopy. --- Analysis, Chemical --- Analytical chemistry --- Chemical analysis --- Metallurgical analysis --- Mineralogy, Determinative --- Radiation monitoring --- Radiometry --- Electromagnetic measurements --- Surfaces (Physics). --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Optics --- Physics --- Surface chemistry --- Surfaces (Technology) --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectroscopy --- Interferometry --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Qualitative --- Spectrometry --- Material science --- Physical sciences
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This book focuses on the metallic Nano- and Micro-materials (NMMs) fabricated by physical techniques such as atomic diffusion. A new technology for fabricating NMMs by atomic diffusion is presented. Two kinds of atomic diffusion are treated; one is a phenomenon caused by electron flow in high density and called electromigration and the other is stress migration which depends on a gradient of hydrostatic stress in a material. In three parts, the book describes the theory of atomic diffusion, the evaluation of physical properties and the treatment and applications of metallic NMMs. The new methods such as atomic diffusion are expected are expected to be crucial for the fabrication of NMMs in the future and to partially replace methods based on chemical reactions.
Diffusion. --- Metallic composites. --- Nanostructured materials. --- Nanostructured materials --- Chemical & Materials Engineering --- Engineering & Applied Sciences --- Technology - General --- Materials Science --- Metal composites --- Metal matrix composites --- Engineering. --- Solid state physics. --- Spectroscopy. --- Microscopy. --- Nanotechnology. --- Nanotechnology and Microengineering. --- Solid State Physics. --- Spectroscopy and Microscopy. --- Composite materials --- Metals --- Molecular technology --- Nanoscale technology --- High technology --- Construction --- Industrial arts --- Technology --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Optics --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectrometry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Physics --- Solids --- Qualitative --- Analytical chemistry
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X-ray diffraction crystallography for powder samples is a well-established and widely used method. It is applied to materials characterization to reveal the atomic scale structure of various substances in a variety of states. The book deals with fundamental properties of X-rays, geometry analysis of crystals, X-ray scattering and diffraction in polycrystalline samples and its application to the determination of the crystal structure. The reciprocal lattice and integrated diffraction intensity from crystals and symmetry analysis of crystals are explained. To learn the method of X-ray diffraction crystallography well and to be able to cope with the given subject, a certain number of exercises is presented in the book to calculate specific values for typical examples. This is particularly important for beginners in X-ray diffraction crystallography. One aim of this book is to offer guidance to solving the problems of 90 typical substances. For further convenience, 100 supplementary exercises are also provided with solutions. Some essential points with basic equations are summarized in each chapter, together with some relevant physical constants and the atomic scattering factors of the elements.
Crystallography. --- Engineering. --- Materials. --- Surfaces (Physics). --- X-ray crystallography --- Chemical & Materials Engineering --- Engineering & Applied Sciences --- Materials Science --- X-ray crystallography. --- Materials science. --- Solid state physics. --- Spectroscopy. --- Microscopy. --- Nanotechnology. --- Materials Science. --- Characterization and Evaluation of Materials. --- Nanotechnology and Microengineering. --- Solid State Physics. --- Spectroscopy and Microscopy. --- Crystallography --- Crystallography and Scattering Methods. --- Construction --- Industrial arts --- Technology --- Leptology --- Physical sciences --- Mineralogy --- Physics --- Surface chemistry --- Surfaces (Technology) --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectrometry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Optics --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Solids --- Molecular technology --- Nanoscale technology --- High technology --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Material science --- Qualitative --- Analytical chemistry
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The high time-resolution radio sky represents unexplored astronomical territory. This thesis presents a study of the transient radio sky, focussing on millisecond scales. As such, the work is concerned primarily with neutron stars. In particular this research concentrates on a recently identified group of neutron stars, known as RRATs, which exhibit radio bursts every few minutes to every few hours. After analysing neutron star birthrates, a re-analysis of the Parkes Multibeam Pulsar Survey is described which has resulted in the discovery of 19 new transient radio sources. Of these, 12 have been seen to repeat and a followup campaign of observations has been undertaken. These studies have greatly increased our knowledge of the rotational properties of RRATs and enable us to conclude that they are pulsars with extreme nulling and/or pulse-to-pulse modulation. Although the evolution of neutron stars post-supernova is not yet understood, it seems that RRATs fit into the emerging picture in which pulsar magnetospheres switch between stable configurations.
Astronomy. --- Radiation sources. --- Radio astronomy. --- Radio waves. --- Astronomy & Astrophysics --- Physical Sciences & Mathematics --- Astrophysics --- Astronomy - General --- Hertzian waves --- Sources of radiation --- Radioastronomy --- Physics. --- Astrophysics. --- Cosmology. --- Spectroscopy. --- Microscopy. --- Astronomy, Astrophysics and Cosmology. --- Spectroscopy and Microscopy. --- Electric waves --- Electromagnetic waves --- Radio frequency --- Radio meteorology --- Signal theory (Telecommunication) --- Quantum optics --- Radiation --- Astronomy --- Interstellar communication --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Optics --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectrometry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Astronomical physics --- Cosmic physics --- Physics --- Qualitative --- Analytical chemistry
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This book provides a comprehensive review of the present status of achievements in the area of soft X-ray laser sources, supplemented by information about sources based on relativistic laser˗matter interaction and their future, and incoherent sources within a very broad spectral range. The diversity of demonstrated or planned applications presented in the book supports the thesis that such sources have now reached a mature stage of development. There is a significant effort worldwide to develop very bright, ultra-short duration, radiation sources in the extreme ultraviolet and X-ray spectral regions, driven by a diversity of potential applications in nearly all branches of science. This book updates the status in this field and focuses on developments in laser plasma-based methods. The scheme of transient inversion proves its robustness by being dominant in the area of repetitive X-ray lasers pumped at grazing-incidence-geometry by optical lasers of moderate energy at increasing repetition rates – these characteristics enable them to be used in university-class laboratories. Experimental and theoretical progress associated with the seeding technique by high harmonics is well covered. This technique is important as it is also considered from the perspective of seeding X-ray free electron lasers. Dramatic progress in laser development and extending the available power range to the petawatt level is stimulating a new generation of methods of ultra-bright and ultra-short pulses of energetic X-rays. These methods, as well as some elements of attoscience based on high harmonics generation, are well represented. Finally, a comprehensive survey of possible applications of the described sources in different areas of science constitutes, by defining the parameter set of interest, a framework for considering the direction further developments will take.
Free electron lasers. --- Ultraviolet radiation. --- X-ray lasers -- Congresses. --- X-ray lasers. --- X-ray lasers --- Physics --- Engineering & Applied Sciences --- Physical Sciences & Mathematics --- Atomic Physics --- Applied Physics --- Physics. --- Atoms. --- Matter. --- Plasma (Ionized gases). --- Spectroscopy. --- Microscopy. --- Atoms and Molecules in Strong Fields, Laser Matter Interaction. --- Plasma Physics. --- Spectroscopy and Microscopy. --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Optics --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectrometry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Gaseous discharge --- Gaseous plasma --- Magnetoplasma --- Ionized gases --- Natural philosophy --- Philosophy, Natural --- Physical sciences --- Dynamics --- Chemistry, Physical and theoretical --- Matter --- Stereochemistry --- Qualitative --- Constitution --- Analytical chemistry
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This volume describes an impressive array of the current photonic-related technologies being used in the investigation of biological systems. The topics include various types of microscopy (fluorescence correlation microscopy, two-photon microscopy), sensitive detection of biological molecules, nano-surgery techniques, fluorescence resonance energy transfer, nano-plasmonics, terahertz spectroscopy, and photosynthetic energy conversion. The emphasis is on the physical principles behind each technique, and on examining the advantages and limitations of each.The book begins with an overview by Paras Prasad, a leader in the field of biophotonics, of several important optical techniques currently used for studying biological systems. In the subsequent chapters these techniques are discussed in depth, providing the reader with a detailed understanding of the basic physical principles at work. An excellent treatment of terahertz spectroscopy demonstrates how photonics is being extended beyond the visible region. Recent results in the use of femtosecond lasers as a tool to porate cell walls demonstrate that the manipulation of light can be used as a tool for the study and the treatment of biological systems. The field of Bio-photonics is broad and still growing, so cannot be covered comprehensively in one volume. But here the reader will find an introduction to some of the major tools used for studying biological systems, and at the same time a detailed, first-principles treatment of the physics behind these tools.
Photobiochemistry --- Photobiology --- Bioorganic photochemistry --- Biophotochemistry --- Chemistry. --- Biotechnology. --- Atoms. --- Physics. --- Biophysics. --- Biological physics. --- Spectroscopy. --- Microscopy. --- Biomaterials. --- Biophysics and Biological Physics. --- Spectroscopy and Microscopy. --- Atomic, Molecular, Optical and Plasma Physics. --- Organic photochemistry --- Biological and Medical Physics, Biophysics. --- Biocompatible materials --- Biomaterials --- Medical materials --- Medicine --- Biomedical engineering --- Materials --- Biocompatibility --- Prosthesis --- Chemical engineering --- Genetic engineering --- Bioartificial materials --- Hemocompatible materials --- Natural philosophy --- Philosophy, Natural --- Physical sciences --- Dynamics --- Chemistry, Physical and theoretical --- Matter --- Stereochemistry --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Optics --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectrometry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Biological physics --- Biology --- Medical sciences --- Physics --- Constitution --- Qualitative --- Analytical chemistry --- Photonics
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Terahertz science and technology is attracting great interest due to its application in a wide array of fields made possible by the development of new and improved terahertz radiation sources and detectors. This book focuses on the development and characterization of one such source - namely the semi-large aperture photoconducting (PC) antenna fabricated on Fe-doped bulk Ga0.69In0.31As substrate. The high ultrafast carrier mobility, high resistivity, and subpicosecond carrier lifetime along with low bandgap make Ga0.69In0.31As an excellent candidate for PC antenna based THz emitter that can be photoexcited by compact Yb-based multiwatt laser systems for high power THz emission. The research is aimed at evaluating the impact of physical properties of a semi-large aperture Ga0.69In0.31As PC antenna upon its THz generation efficiency, and is motivated by the ultimate goal of developing a high-power terahertz radiation source for time-domain terahertz spectroscopy and imaging systems. This Doctoral Thesis has been accepted by Rensselaer Polytechnic Institute, Troy, USA.
Femtochemistry. --- Millimeter wave devices. --- Optoelectronic devices. --- Submillimeter waves. --- Terahertz technology. --- Submillimeter waves --- Physics --- Physical Sciences & Mathematics --- Light & Optics --- Electricity & Magnetism --- Microwave spectroscopy. --- Photo electric devices --- Photo electronic devices --- Photoelectronic devices --- Submillimeter radiation --- Submillimeter-terahertz radiation --- Terahertz radiation --- Waves, Submillimeter --- Physics. --- Semiconductors. --- Lasers. --- Photonics. --- Spectroscopy. --- Microscopy. --- Optical materials. --- Electronic materials. --- Spectroscopy and Microscopy. --- Laser Technology, Photonics. --- Optical and Electronic Materials. --- Molecular spectroscopy --- Radiofrequency spectroscopy --- Electronic apparatus and appliances --- Optical instruments --- Electrooptical devices --- Integrated optics --- Electromagnetic waves --- Radiation --- Optics, Lasers, Photonics, Optical Devices. --- Optics --- Materials --- Electronic materials --- New optics --- Light amplification by stimulated emission of radiation --- Masers, Optical --- Optical masers --- Light amplifiers --- Light sources --- Optoelectronic devices --- Nonlinear optics --- Optical parametric oscillators --- Crystalline semiconductors --- Semi-conductors --- Semiconducting materials --- Semiconductor devices --- Crystals --- Electrical engineering --- Electronics --- Solid state electronics --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Qualitative --- Spectrometry --- Analytical chemistry
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Within the last 30 years, electron energy-loss spectroscopy (EELS) has become a standard analytical technique used in the transmission electron microscope to extract chemical and structural information down to the atomic level. In two previous editions, Electron Energy-Loss Spectroscopy in the Electron Microscope has become the standard reference guide to the instrumentation, physics and procedures involved, and the kind of results obtainable. Within the last few years, the commercial availability of lens-aberration correctors and electron-beam monochromators has further increased the spatial and energy resolution of EELS. This thoroughly updated and revised Third Edition incorporates these new developments, as well as advances in electron-scattering theory, spectral and image processing, and recent applications in fields such as nanotechnology. The appendices now contain a listing of inelastic mean free paths and a description of more than 20 MATLAB programs for calculating EELS data. Considered the "Bible of EELS" Presents the only in-depth, single-author text for the still-expanding field of TEM-EELS Responds to many requests for the first new edition of this classic work since 1996 Includes discussion of new spectrometer and detector designs, together with spectral-analysis techniques such as Bayesian deconvolution and multivariate statistical analysis Provides extended discussion of anisotropic materials, retardation effects, delocalization of inelastic scattering, and the simulation of energy-loss fine structure. Describes recent applications of EELS to fields such as nanotechnology, electronic devices and carbon-based materials. Offers extended coverage of radiation damage and delocalization as limits to spatial resolution. From reviews of the first and second edition: "The text....contains a wealth of practical detail and experimental insight....This book is an essential purchase for any microscopist who is using, or planning to use, electron spectroscopy or spectroscopic imaging." – JMSA "Provides the advanced student with an indispensable text and the experienced researcher with a valuable reference." -- American Scientist.
Electron microscopy. --- Electrons. --- Energy. --- Spectroscopy. --- Electron energy loss spectroscopy --- Electron microscopy --- Chemical & Materials Engineering --- Physics --- Engineering & Applied Sciences --- Physical Sciences & Mathematics --- Materials Science --- Light & Optics --- Electron energy loss spectroscopy. --- EELS (Spectrum analysis) --- Energy loss spectroscopy, Electron --- Spectroscopy, Electron energy loss --- Materials science. --- Solid state physics. --- Microscopy. --- Nanotechnology. --- Materials Science. --- Characterization and Evaluation of Materials. --- Spectroscopy/Spectrometry. --- Spectroscopy and Microscopy. --- Solid State Physics. --- Molecular technology --- Nanoscale technology --- High technology --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Optics --- Solids --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Material science --- Physical sciences --- Qualitative --- Microscopy --- Electron spectroscopy --- Surfaces (Physics). --- Surface chemistry --- Surfaces (Technology) --- Spectrometry --- Analytical chemistry
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Microscopy plays an integral role in the research and development of new medicines. Pharmaceutical Microscopy describes a wide variety of techniques together with numerous practical applications of importance in drug development. The first section presents general methods and applications with an emphasis on the physical science aspects. Techniques covered include optical crystallography, thermal microscopy, scanning electron microscopy, energy dispersive x-ray spectrometry, microspectroscopy (infrared and Raman), and particle size and shape by image analysis. The second section presents applications of these techniques to specific topics of pharmaceutical interest, including studies of polymorphism, particle size and shape analysis, and contaminant identification. Pharmaceutical Microscopy is designed for those scientists who must use these techniques to solve pharmaceutical problems but do not need to become expert microscopists. Consequently, each section has exercises designed to teach the reader how to use and apply the techniques in the book. Although the focus is on pharmaceutical development, workers in other fields such as food science and organic chemistry will also benefit from the discussion of techniques and the exercises. Provides comprehensive coverage of key microscopy techniques used in pharmaceutical development Helps the reader to solve specific problems in pharmaceutical quality assurance Oriented and designed for pharmaceutical scientists who need to use microscopy but are not expert microscopists Includes a large number of practical exercises to give the reader hands-on experience with the techniques Written by an author with 21 years of experience in the pharmaceutical industry.
Chemistry. --- Drug development. --- Drug discovery. --- Food science. --- Microscopy. --- Pharmaceutical technology. --- Spectroscopy. --- Microscopy --- Drug development --- Investigative Techniques --- Optics and Photonics --- Diagnostic Imaging --- Chemistry, Pharmaceutical --- Pharmacology --- Diagnostic Techniques and Procedures --- Analytical, Diagnostic and Therapeutic Techniques and Equipment --- Physics --- Chemistry --- Natural Science Disciplines --- Diagnosis --- Biological Science Disciplines --- Disciplines and Occupations --- Drug Discovery --- Biology --- Health & Biological Sciences --- Physical Sciences & Mathematics --- Analytical Chemistry --- Technique --- Analysis, Microscopic --- Light microscopy --- Micrographic analysis --- Microscope and microscopy --- Microscopic analysis --- Optical microscopy --- Food --- Materials science. --- Spectroscopy/Spectrometry. --- Pharmaceutical Sciences/Technology. --- Characterization and Evaluation of Materials. --- Food Science. --- Biological Microscopy. --- Spectroscopy and Microscopy. --- Biotechnology. --- Optics --- Surfaces (Physics). --- Surface chemistry --- Surfaces (Technology) --- Pharmaceutical laboratory techniques --- Pharmaceutical laboratory technology --- Technology, Pharmaceutical --- Technology --- Science --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Qualitative --- Spectrometry --- Food—Biotechnology. --- Material science --- Physical sciences --- Analytical chemistry
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