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The purpose of this volume is to show how in this area the technology, creativity and inventiveness are the basis of new and encouraging results not only in the environmental field but also in the monitoring of xenobiotics of organic and inorganic origin in complex matrices. The final objective will always be on determining the fundamental parameters of interest to set up an analytical procedure, such as precision and trueness (that together give accuracy), the limits of detection and quantification, selectivity, and especially sensitivity, or attempting to increase this

azides --- screen-printed sensors --- poly (3-octylthiophene) --- solid contact potentiometric sensors --- iron-phthalocyanine --- nitron-azide complexes --- microwave-assisted aqueous two-phase extraction --- Solasodine --- alkaloid --- response surface methodology --- high-performance liquid chromatography --- pre-development process --- clotrimazole --- itraconazole --- stability --- method validation --- sporotrichosis --- differential pulse voltammetry --- hydrochlorothiazide --- pyridoxine --- chemometrics --- bioindication --- heavy metals --- urban soil --- Senecio vulgaris --- Poa annua --- Polygonum aviculare --- predictive models --- MIPs --- parabens --- biological matrix --- extraction procedure --- HPLC-PDA --- stationary phase characterization --- phenol --- 3-aminophenol --- wastewater --- SPMMTE --- capillary electrophoresis --- deoxynivalenol --- dcELISA kit --- performance measurement --- development --- grapevine --- bioaccumulation --- biomonitoring --- laser-induced breakdown spectroscopy --- surface pollution --- high voltage insulators --- quantitatively analysis