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This book is a collection of 13 innovative papers describing the state of the art and the future perspectives in solid-phase extraction covering several analytical fields prior to the use of gas or liquid chromatographic analysis. New sorptive materials are presented including carbon nanohorn suprastructures on paper support, melamine sponge functionalized with urea–formaldehyde co-oligomers, chiral metal–organic frameworks, UiO-66-based metal–organic frameworks, and fabric phase sorptive media for various applications. Solid-phase extraction can be applied in several formats aside from the conventional cartridges or mini-column approach, e.g., online solid-phase extraction, dispersive solid-phase microextraction, and in-syringe micro-solid-phase extraction can be very helpful for analyte pre-concentration and sample clean-up. Polycyclic musks in aqueous samples, 8-Nitroguanine in DNA by chemical derivatization antibacterial diterpenes from the roots of salvia prattii, perfluoroalkyl substances (PFASs) in aater samples by bamboo charcoal-based SPE, parabens in environmental water samples, benzotriazoles as environmental pollutants, organochlorine pesticide residues in various fruit juices and water samples and synthetic peptide purification are among the applications cited in this collection. All these outstanding contributions highlight the necessity of this analytical step, present the advantages and disadvantages of each method and focus on the green analytical chemistry guidelines that have to be fulfilled in current analytical practices.

method validation --- nitrated DNA lesion --- benzotriazoles --- microextraction --- LC-MS/MS --- perfluoroalkyl acids --- antibacterial diterpenes --- in-house loaded SPE --- isotope-dilution --- polycyclic musks --- wastewater --- peptide --- HPLC-DAD --- chiral compounds --- derivatization --- extraction --- water --- enantiomeric excess --- sample preparation --- metal-organic frameworks --- solid-phase extraction --- FPSE --- melamine sponge --- preparative high-performance liquid chromatography --- GC–MS/MS --- solid phase peptide synthesis --- HPLC-PDA --- Salvia prattii --- in-syringe micro solid-phase extraction --- organochlorine pesticides --- hydrophilic solid-phase extraction --- response surface methodology --- IBD --- graphene --- sorptive phase --- paper --- liquid chromatography–tandem mass spectrometry --- carbon nanohorns --- gradient elution --- peroxynitrite --- bamboo charcoal --- gas chromatography-mass spectrometry --- environmental samples --- parabens --- solid phase extraction (SPE) --- preparative purification --- antidepressants --- online solid-phase extraction --- organic pollutants --- urea-formaldehyde co-oligomers --- personal care products --- dispersive solid-phase extraction --- fabric phase sorptive extraction --- analyte partitioning