TY - BOOK ID - 145729609 TI - Five Years of Separations : Feature Paper 2018 AU - Samanidou, Victoria AU - Lucena, Rafael PY - 2020 PB - Basel, Switzerland MDPI - Multidisciplinary Digital Publishing Institute DB - UniCat KW - Research & information: general KW - recycled diatomaceous earth KW - solid phase microextraction KW - polycyclic aromatic hydrocarbons KW - gas chromatography-mass spectrometry KW - antibody-drug conjugate KW - biopharmaceutical KW - cytotoxicity KW - hydrophobicity KW - micellar electrokinetic chromatography KW - tandem mass spectrometry KW - linear ion trap KW - glycolipid KW - diacyltrehalose KW - Mycobacterium tuberculosis KW - bisphosphonates KW - risedronate KW - zoledronate KW - tiludronate KW - ZIC-HILIC KW - PDA KW - quantitation KW - tablets KW - ionic liquid stationary phase KW - gas chromatography KW - chromatographic selectivity KW - alkylated polycyclic aromatic hydrocarbons (alkylated PAHs) KW - diphenylamine KW - gunshot residues KW - hands KW - dry cotton swab KW - in-tube solid-phase extraction KW - capillary liquid chromatography KW - SEM-EDX KW - thyroid KW - dissolution KW - liquid chromatography-mass spectrometry KW - membrane filtration-treatment KW - membrane type-operation KW - membrane fouling mechanism KW - tannery industrial wastewater KW - vibratory shear-enhanced process (VSEP) KW - tricyclic antidepressants (TCAs) KW - sample treatment KW - biological fluids KW - UV filters KW - matrix solid-phase dispersion KW - μ-MSPD KW - miniaturized extraction technique KW - GC–MS/MS KW - cosmetic analysis KW - personal care products KW - fragrance allergens KW - preservatives KW - plasticizers KW - synthetic musks KW - recycled diatomaceous earth KW - solid phase microextraction KW - polycyclic aromatic hydrocarbons KW - gas chromatography-mass spectrometry KW - antibody-drug conjugate KW - biopharmaceutical KW - cytotoxicity KW - hydrophobicity KW - micellar electrokinetic chromatography KW - tandem mass spectrometry KW - linear ion trap KW - glycolipid KW - diacyltrehalose KW - Mycobacterium tuberculosis KW - bisphosphonates KW - risedronate KW - zoledronate KW - tiludronate KW - ZIC-HILIC KW - PDA KW - quantitation KW - tablets KW - ionic liquid stationary phase KW - gas chromatography KW - chromatographic selectivity KW - alkylated polycyclic aromatic hydrocarbons (alkylated PAHs) KW - diphenylamine KW - gunshot residues KW - hands KW - dry cotton swab KW - in-tube solid-phase extraction KW - capillary liquid chromatography KW - SEM-EDX KW - thyroid KW - dissolution KW - liquid chromatography-mass spectrometry KW - membrane filtration-treatment KW - membrane type-operation KW - membrane fouling mechanism KW - tannery industrial wastewater KW - vibratory shear-enhanced process (VSEP) KW - tricyclic antidepressants (TCAs) KW - sample treatment KW - biological fluids KW - UV filters KW - matrix solid-phase dispersion KW - μ-MSPD KW - miniaturized extraction technique KW - GC–MS/MS KW - cosmetic analysis KW - personal care products KW - fragrance allergens KW - preservatives KW - plasticizers KW - synthetic musks UR - https://www.unicat.be/uniCat?func=search&query=sysid:145729609 AB - Five years of Separations are celebrated by a collection of ten feature articles: one review and nine research articles on topics of current interest. Applications of Gas Chromatography for the Analysis of Tricyclic Antidepressants in Biological Matrices are presented focusing on novel extraction techniques and novel materials used for sample preparation due to the great demand for method development for the determination of TCAs in biofluids, especially for therapeutic drug monitoring. Original research articles include the following: 1. Insights into the Mechanism of Separation of Bisphosphonates by Zwitterionic Hydrophilic Interaction Liquid Chromatography: Application to the Quantitation of Risedronate in Pharmaceuticals. 2. A method based on micro-matrix solid-phase dispersion (μ-MSPD) followed by gas-chromatography tandem mass spectrometry (GC–MS/MS), developed to analyze UV filters in personal care products. 3. The performance of a vibratory shear-enhanced process (VSEP) combined with an appropriate membrane unit for the treatment of simulated or industrial tannery wastewaters. 4. A method for the analysis of thyroid hormones by liquid chromatography-mass spectrometry that was used for the dissolution testing of single- and dual-component thyroid hormone supplements via a two-stage biorelevant dissolution procedure. 5. A method involving the collection and determination of organic and inorganic gunshot residues on hands using online in-tube solid-phase microextraction (IT-SPME) coupled to miniaturized capillary liquid chromatography with diode array detection (CapLC-DAD) and scanning electron microscopy coupled to energy dispersion X-ray (SEM-EDX), respectively, for quantifying both residues. 6. The gas chromatographic retention behavior of 16 polycyclic aromatic hydrocarbons (PAHs) and alkylated PAHs on a new ionic liquid stationary phase, 1,12-di(tripropylphosphonium) dodecane bis(trifluoromethanesulfonyl)imide (SLB®-ILPAH) intended for the separation of PAH mixtures, which was compared with the elution pattern on more traditional stationary phases: a non-polar phenyl arylene (DB-5ms) and a semipolar 50% phenyl dimethyl siloxane (SLB PAHms) column. 7. The Multiple-Stage Precursor Ion Separation and High Resolution Mass Spectrometry toward Structural Characterization of 2,3-Diacyltrehalose Family from Mycobacterium tuberculosis 8. The use of micellar electrokinetic chromatography (MEKC) for studying the hydrophobic character of modified Monomethyl Auristatin E derivatives, as Novel Candidates for the Design of Antibody–Drug Conjugates, which are promising state-of-the-art biopharmaceutical drugs for selective drug-delivery applications and the treatment of diseases such as cancer. 9. The use of recycled diatomaceous earth as the extraction phase in solid phase microextraction (SPME) technique for the determination of polycyclic aromatic hydrocarbons (PAHs) in river water samples, with separation/detection performed by gas chromatography-mass spectrometry (GC-MS). ER -